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. 2023 Mar 2;28(5):2328. doi: 10.3390/molecules28052328

Figure 1.

Figure 1

ORTEP drawing of complex 5b with thermal ellipsoid plot shown at 50% probability level. Hydrogen atoms and PF6 counterions have been omitted for clarity. Selected bond distances (Å) and angles (˚) for 5b: Pd(1)-C(1) 2.080(3), Pd(1)-P(1) 2.3098(8), Pd(1)-P(2) 2.2762(8), Pd(1)-P(3) 2.3334(8), P(2)-Pd(1)-P(1) 83.97(3), P(2)-Pd(1)-P(3) 83.48(3) P(1)-Pd(1)-P(3) 163.65(3), C(1)-Pd(1)-P(3) 97.36(8), C(1)-Pd(1)-P(2) 176.84(9), C(1)-Pd(1)-P(1) C6 Pd1 P1 94.63(8). Selected crystallographic data: a, 13.1305(4); b, 14.8772(4); c, 20.4043(7) Å. β, 102.551(1)°. Volume 3890.6(2) Å3. Z = 2. 2Θ range for data collection/° 4.92 to 52.74. Reflections collected, 50817. Independent reflections, 7952 [Rint = 0.0481, Rsigma = 0.0303]. Final R indexes [I > = 2σ (I)] R1 = 0.0407, wR2 = 0.0891. Final R indexes [all data] R1 = 0.0501, wR2 = 0.0937.