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. 2023 Mar 17;13(13):8890–8900. doi: 10.1039/d2ra07510e

Optimizing the best conditions for the synthesis of tetrazoles in the presence of Co-(PYT)2@BNPs nanocatalyst.

Entry Amount of the catalyst (mg) Solvent NaN3 (mmol) Time (min) Temperature (°C) Yield (%)a
1 PEG 1.4 150 120 N. R.b
2 40 PEG 1.4 310 120 85
3 50 PEG 1.4 100 120 98
4 50 PEG 1.3 120 120 80
5 50 DMSO 1.4 100 120 81
6 50 H2O 1.4 100 Reflux 20
7 50 PEG 1.4 100 100 49
a

Isolated yield within 120 min.

b

No reaction.