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. 2023 Mar 11;12(6):1188. doi: 10.3390/foods12061188

Table 3.

Conditions of chromatographic analysis.

Carrier Gas Helium 6.0 from SIAD (Ruda Śląska, Poland)
Injection velocity 3 mL/min
Injection temperature 250 °C 325 °C
Column Type SLBTM—5 ms HP—5ms
Column size 30 m × 0.25 mm
Column film thickness 0.25 μm
Oven temperature
program
80 °C held for 6 min 40 °C for 2 min
5 °C/min up to 260 °C
20 °C/min up to 300 °C
held for 2 min
10 °C/min up to 300 °C
held 10 min
Transfer line temperature 250 °C 325 °C
Ion trap temperature 150 °C
Ion source temperature 230 °C
Ion registration mode TIC
Ion registration range (m/z) 50 ÷ 600