Table 3.
Conditions of chromatographic analysis.
Carrier Gas | Helium 6.0 from SIAD (Ruda Śląska, Poland) | |
---|---|---|
Injection velocity | 3 mL/min | |
Injection temperature | 250 °C | 325 °C |
Column Type | SLBTM—5 ms | HP—5ms |
Column size | 30 m × 0.25 mm | |
Column film thickness | 0.25 μm | |
Oven temperature
program |
80 °C held for 6 min | 40 °C for 2 min |
5 °C/min up to 260 °C | ||
20 °C/min up to 300 °C held for 2 min |
10 °C/min up to 300 °C held 10 min |
|
Transfer line temperature | 250 °C | 325 °C |
Ion trap temperature | 150 °C | |
Ion source temperature | 230 °C | |
Ion registration mode | TIC | |
Ion registration range (m/z) | 50 ÷ 600 |