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. 2023 Mar 8;24(6):5170. doi: 10.3390/ijms24065170

Figure 7.

Figure 7

GPC traces of poly(β-pinene)s obtained at different polymerization times by the TMPCl/TiCl4/TMEDA initiating system in DCM/hexane (45/55 v/v%) solvent mixture at room temperature ([TMPCl]/[Pin]/[TiCl4]/[TMEDA] = 1/73/10/1; [TMPCl] = 0.01 M; * after 60 min reaction time a second feed of monomer was added to the reaction mixture).