Figure 11.
1H NMR spectrum of poly(β-pinene) synthesized by the TMPCl/TiCl4/TMEDA initiating system in DCM/hexane (45/55 v/v%) solvent mixture at −78 °C ([TMPCl]/[Pin]/[TiCl4]/[TMEDA] = 1/73/10/1; [TMPCl] = 0.01 M; reaction time: 60 min).
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