Table 2.
Levels selected for each factor for the validation assays of ethanol and acetone extraction models and respective experimental (mean ± standard deviation) and predicted responses.
T (°C) | t (h) | L/S (mL/g Dry GP) | Solvent (%) | TPh (mg GAE/g Dry GP) | |
---|---|---|---|---|---|
Experimental | Predicted | ||||
Ethanol extraction | |||||
60 | 1.50 | 25 | 50 | 40.4 ± 1.8 | 43. 6 |
50 | 1.50 | 25 | 50 | 34.4 ± 1.0 | 36.6 |
50 | 1.25 | 15 | 30 | 28.3 ± 2.9 | 27.2 |
40 | 0.75 | 15 | 30 | 20.6 ± 0.1 | 21.7 |
50 | 1.00 | 20 | 70 | 27.5 ± 0.01 | 30.0 |
Acetone extraction | |||||
50 | 1.50 | 25 | 50 | 54. 6 ± 3.4 | 55.6 |
40 | 1.50 | 25 | 50 | 49.4 ± 0.9 | 48.9 |
45 | 1.25 | 15 | 30 | 35.9 ± 1.4 | 38.2 |
35 | 0.75 | 15 | 30 | 34.9 ± 0.6 | 34.7 |
40 | 1.00 | 20 | 70 | 40.9 ± 4.1 | 40.4 |
T—temperature; t—time; L/S—liquid–solid ratio; TPh—total phenolic content; GAE—gallic acid equivalents; GP—grape pomace.