1st step | −50 °C | 150 mTorr | 2 h |
2nd step | −40 °C | 100 mTorr | 2 h |
3rd step | −30 °C | 100 mTorr | 2 h |
4th step | −20 °C | 50 mTorr | 2 h |
5th step | −10 °C | 50 mTorr | 2 h |
6th step | −5 °C | 50 mTorr | 2 h |
7th step | 0 °C | 50 mTorr | 2 h |
8th step | +10 °C | 50 mTorr | 2 h |
9th step | +20 °C | 50 mTorr | 4 h |