Table 2.
Sample | NMR Data (ppm) | ||||||||
---|---|---|---|---|---|---|---|---|---|
C=O | CH3 | C1 | C2 | C3 | C4 | C5 | C6 | ||
COS–3 | GlcN″ | 100.4 | 58.5 | 74.4 | 72.3 | 79.1 | 62.9 | ||
GlcN′ | 100.2 | 58.5 | 79.1 | 77.4 | 72.8 | 62.7 | |||
GlcNβ | 95.3 | 59.3 | 70.6 | 79.1 | 72.6 | 62.7 | |||
GlcNα | 91.6 | 56.9 | 70.6 | 79.1 | 72.6 | 62.7 | |||
N–3 | GlcNAc″ | 174.8 | 22.6 22.5 22.3 |
101.8 | 56.0 | 73.9 | 70.1 | 76.3 | 61.0 |
GlcNAc′ | 101.6 | 55.4 | 72.6 | 79.6 | 74.9 | 60.4 | |||
GlcNAcβ | 95.2 | 56.5 | 72.9 | 79.6 | 75.0 | 60.5 | |||
GlcNAcα | 90.8 | 54.1 | 69.6 | 80.1 | 70.4 | 60.4 |