Table 1.
Compound 1 | Compound 2 | |||||
---|---|---|---|---|---|---|
Position | ẟ C | ẟ H | HMBC | ẟ C | ẟ H | HMBC |
2 | 152.5 | 7.80 | 3, 4, 8a, 1′ | 152.0 | 7.94 | 3, 4, 8a, 1′ |
3 | 122.5 | - | 124.3 | - | ||
4 | 175.0 | - | 175.9 | - | ||
4a | 113.7 | - | 118.4 | - | ||
5 | 153.0 | - | 127.8 | 8.22 | 4, 7, 8, 8a | |
6 | 152.9 | - | 115.0 | 7.01 | 8, 4a | |
7 | 157.6 | - | 163.2 | - | ||
8 | 96.1 | 6.72 | 4, 6, 7 | 100.9 | 6.88 | 7, 4a, 8a |
8a | 154.6 | - | 157.9 | - | ||
1′ | 112.8 | - | 124.9 | - | ||
2′ | 140.5 | - | 130.2 | 7.52 | 3, 3′, 4′ | |
3′ | 95.3 | 6.63 | 2′, 4′, 5′ | 114.0 | 6.99 | 1′, 2′, 4′, 5′ |
4′ | 148.4 | - | 159.6 | - | ||
4′-OMe | - | - | 55.4 | 3.86 | 4′ | |
5′ | 141.1 | - | 114.0 | 6.99 | 1′, 2′, 4′, 5′ | |
6′ | 111.4 | 6.85 | 2′, 4′, 5′ | 130.2 | 7.52 | 3, 3′, 4′ |
O-CH2-O | 101.3 | 5.97 | 4′, 5′ | - | - | |
5-OMe | 56.3 | 3.98 | 5 | - | - | |
6-OMe | 56.8 | 3.75 | 6 | - | - | |
7-OMe | 62.1 | 3.97 | 6, 7 | - | - | |
2′-OMe | 61.6 | 3.93 | 2′ | - | - | |
1″ | - | - | 65.5 | 4.66 | 7, 2″, 3″ | |
2″ | - | - | 119.3 | 5.55 | 3″-Me, 3″, 4″ | |
3″ | - | - | 141.1 | - | ||
3″-Me | - | - | 16.8 | 1.78 | 2″, 3″, 4″ | |
4″ | - | - | 42.2 | 2.82 | 2″, 3″-Me, 6″ | |
5″ | - | - | 140.5 | 5.70 | 4″, 6″, 7″ | |
6″ | - | - | 123.9 | 5.66 | 4″ | |
7″ | - | - | 70.7 | - | ||
8″ | - | - | 29.9 | 1.35 | 6″, 7″ |