Skip to main content
. 2023 Mar 21;28(6):2846. doi: 10.3390/molecules28062846

Table 1.

1H-(500 MHz) and 13C (125 MHz) NMR spectroscopic data of 1 and 2 recorded in CDCl3 ( in ppm).

Compound 1 Compound 2
Position C H HMBC C H HMBC
2 152.5 7.80 3, 4, 8a, 1′ 152.0 7.94 3, 4, 8a, 1′
3 122.5 - 124.3 -
4 175.0 - 175.9 -
4a 113.7 - 118.4 -
5 153.0 - 127.8 8.22 4, 7, 8, 8a
6 152.9 - 115.0 7.01 8, 4a
7 157.6 - 163.2 -
8 96.1 6.72 4, 6, 7 100.9 6.88 7, 4a, 8a
8a 154.6 - 157.9 -
1′ 112.8 - 124.9 -
2′ 140.5 - 130.2 7.52 3, 3′, 4′
3′ 95.3 6.63 2′, 4′, 5′ 114.0 6.99 1′, 2′, 4′, 5′
4′ 148.4 - 159.6 -
4′-OMe - - 55.4 3.86 4′
5′ 141.1 - 114.0 6.99 1′, 2′, 4′, 5′
6′ 111.4 6.85 2′, 4′, 5′ 130.2 7.52 3, 3′, 4′
O-CH2-O 101.3 5.97 4′, 5′ - -
5-OMe 56.3 3.98 5 - -
6-OMe 56.8 3.75 6 - -
7-OMe 62.1 3.97 6, 7 - -
2′-OMe 61.6 3.93 2′ - -
1″ - - 65.5 4.66 7, 2″, 3″
2″ - - 119.3 5.55 3″-Me, 3″, 4″
3″ - - 141.1 -
3″-Me - - 16.8 1.78 2″, 3″, 4″
4″ - - 42.2 2.82 2″, 3″-Me, 6″
5″ - - 140.5 5.70 4″, 6″, 7″
6″ - - 123.9 5.66 4″
7″ - - 70.7 -
8″ - - 29.9 1.35 6″, 7″