表4.
尿液中7种苯系物代谢物在3个加标水平下的回收率和日内、日间精密度(n=6)
| Compound | Spiked/ (μg/L) |
Recovery/ % |
Intra-day precision/% |
Inter-day precision/% |
|---|---|---|---|---|
| MU | 10.0 | 113 | 3.5 | 7.1 |
| 100 | 106 | 2.0 | 5.7 | |
| 1000 | 104 | 3.9 | 4.5 | |
| PMA | 0.2 | 105 | 4.9 | 7.9 |
| 2.0 | 101 | 6.3 | 3.3 | |
| 20 | 108 | 8.6 | 1.9 | |
| BMA | 2.0 | 104 | 2.8 | 7.6 |
| 20.0 | 103 | 1.8 | 3.0 | |
| 200 | 105 | 3.2 | 3.5 | |
| HA | 1000 | 86 | 5.0 | 21.4 |
| 10000 | 84 | 3.6 | 14.5 | |
| 100000 | 85 | 2.8 | 6.1 | |
| 2MHA | 2.0 | 111 | 2.9 | 4.1 |
| 20.0 | 103 | 3.3 | 3.1 | |
| 200 | 106 | 4.7 | 3.2 | |
| 3MHA+4MHA | 2.0 | 109 | 8.2 | 4.1 |
| 20.0 | 123 | 4.2 | 5.4 | |
| 200 | 119 | 7.3 | 4.7 |