X-ray crystallography data collection and refinement statistics.
| Apo-ZS (PDB 8F23) | Zn2+-ZS (PDB 8ETB) | |
|---|---|---|
| Crystal parameters | ||
| Space group | P1211 | P1211 |
| a (Å) | 44.050 | 43.834 |
| b (Å) | 68.431 | 68.501 |
| c (Å) | 57.676 | 57.923 |
| α (°) | 90.00 | 90.00 |
| β (°) | 101.00 | 100.79 |
| γ (°) | 90.00 | 90.00 |
| Data collection | ||
| Wavelength (Å) | 0.97918 | 1.28215 |
| Resolution | 1.93 | 1.63 |
| Unique reflections | 25 254 | 79 581 |
| R merge | 0.099 | 0.067 |
| I/σ | 10.4 | 9.49 |
| Completeness (%) | 98.1 | 96.60 |
| Redundancy | 6.8 | 4.0 |
| Refinement | ||
| R/Rfree | 0.1975/0.2266 | 0.1976/0.2341 |
| RMSD | ||
| Bond lengths (Å) | 0.009 | 0.004 |
| Bond angles (°) | 1.070 | 0.671 |
| Dihedral (°) | 15.993 | 14.490 |
| Mean B factors (Å 2 ) | ||
| Protein | 61.49 | 41.72 |
| Solvent | 61.56 | 43.90 |
| Ligand | N/A | 42.61 |
| Ramachandran stats (%) | ||
| Favored | 97.53 | 97.53 |
| Allowed | 2.47 | 2.47 |
| Outliers | 0.00 | 0.00 |