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. Author manuscript; available in PMC: 2023 Nov 16.
Published in final edited form as: J Am Chem Soc. 2022 Oct 31;144(45):20875–20883. doi: 10.1021/jacs.2c09045

Table 3.

Hydroalkenylation/Diastereoselective Rearrangement Cascadea

graphic file with name nihms-1887194-t0004.jpg
a

0.15 mmol scale, 1:2 = 1:2, isolated yields. Conditions C: Xantphos Pd G3 (10 mol %), Xantphos (20 mol %), acetic acid (4 equiv), Et3SiH (2 equiv), TBAB (1 equiv), 1,4-dioxane/toluene (0.15 M), blue LED (40 W, 427 nm), 16 h.