Table 1.
Data | Parameter | Measure |
---|---|---|
Data Collection | accelerating voltage (kV) | 300 |
wavelength (Å) | 0.019687 | |
electron source | field emission gun | |
total accumulated | 0.64 | |
exposure (e^-Å −2) | ||
no. of crystals | 1 | |
microscope | Thermo Fisher Titan Krios | |
camera | Falcon 4 electron counting | |
rotation rate (deg/sec) | 0.2 | |
| ||
Data analysis | resolution range (A) | 30.42–2.10 |
space group | P41212 | |
a, c, c (Å) | 68.26, 68.26, 101.95 | |
α, β, ϒ (°) | 90, 90, 90 | |
reflections, total/unique | 56301/12774 | |
multiplicity | 4.41 | |
completeness (%) | 87.0 | |
mean I/Iσ(I) | 2.82 | |
CC1/2 | 92.5 | |
Rwork | 0.2442 | |
Rfree | 0.2917 |