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Exemplary cyclic voltammetry of Hydroxy‐TEMPO (5) and Oxo‐TEMPO (9). Hydroxy‐TEMPO remains stable under the investigated conditions, the peak of Oxo‐TEMPO drops off with increasing number of performed cycles (10 mM mediator, measured in 0.1 M NaOAc‐buffer, pH 4.5, at a scan rate of 100 mV s−1).
