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Conversion to anis aldehyde after a) 5 h reaction time b) 24 h reaction time; conditions: [Anis alcohol]=20 mM, [Hydroxy‐TEMPO 5]=10 mM (0.5 equiv.), 6 mM (0.3 equiv.=30 mol %), 4 (0.2 equiv.=20 mol %), 2 mM (0.1 equiv.=10 mol %), 1 mM (0.05 equiv.=5 mol %) 0.2 mM (0.025. equiv.=2.5 mol %), activity (T. versicolor)=3 U/mL, 1 atm O2, rt, reaction time: 24 h, reaction monitoring via GC‐FID (internal standard method: methyl benzoate) after 5 h and 24 h reaction time.
