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. 2023 Mar 29;28(7):3060. doi: 10.3390/molecules28073060

Table 1.

Extraction of polyphenols through different modern extraction techniques.

Extraction
Techniques
Vegetal
Materials
Solvent Extraction Ratio Extraction Conditions References
Liquid–liquid
extraction
Olive mill wastewater - Ethyl acetate
Temperature: 25 °C
Extraction time: 20 min
Four extraction cycles
[77]
Solid–liquid
extraction
Olive pomace Solvent-to-feed ratio: 1:5 (w/v)
Ethanol, pH 2
Temperature: 25 °C
Time: 180 min
[78]
UAE Jussara pulp Solvent-to-feed ratio: 20 mL/g
50% ethanol in distilled water
pH 3
Time: 20 min
Temperature: 25 °C
[63]
UAE Grape skins Solvent-to-feed ratio: 1:10 (w/v)
Ethanol: water 50:50 v/v
Temperature: 25 °C
Time: 9 min
[79]
UAE Wine lees Solvent-to-feed ratio: 1:60 (w/v)
Ethanol 43.9%
Temperature: 60 °C
Time: 25 min
[80]
MAE Apple pomace Solvent-to-feed ratio: 22.9:1
Ethanol concentration: 62.1%
Microwave power: 650.4 W
Extraction time: 53.7 s
Temperature: 70 °C
[81]
PLE Grape pomace - Solvent extraction: ethanol: water 50:50 v/v
Temperature: 80 °C
Time: 50 min
Pressure: 100 bar
[82]
EAE Grape seeds Enzyme dosage: 20 mg/g
Water
pH 3.55
Lallzyme EX-V
Enzyme dosage: 20 mg g−1
Temperature: 48 °C
Time: 2.60 h
[83]
EAE Corn husk 1 g plant to 10 mL of 0.1 M PCB at pH 5.0
Cellulase
Incubation: 40 °C
Inactivation of the enzyme in boiling water for 5 min
Solvent extraction: ethanol
Time: 2 h
Temperature: 80 °C
[84]
PEF Cistus creticus 1 g plant in 10 mL solvent PEF treatment time: 20 min
Following extraction step: magnetic stirrer (500 rpm) and heated at 50 °C (in an oil bath) for 3 h
[50]