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. 2023 Apr 12;18(4):e0284186. doi: 10.1371/journal.pone.0284186

Table 4. Experimental conditions.

Test Specimen size Test conditions Test Index
Chloride ion permeability test Φ10 × 5 cm Acceleration voltages: 0V, 20V, and 30V Penetration depth, Content
Antifreezing test 10 cm×10 cm×40 cm Center temperature: - 17 ± 2°C and 8 ± 2°C Temperature range: 6°C to—15°C Mass loss Mechanical property, Stress-strain curve
Mechanical property measurement 10 cm×10 cm×40 cm Loading speed: 2400 ± 200N / s Flexural strength, Compressive strength
Microstructure analysis 1cm × 1cm × 1cm Terminate hydration:48 hours C-S-H gel, CH crystals, Micro-pores and cracks
XRD analysis 1cm × 1cm × 1cm Test radius: ≥ 200 mm, Scanning speed: 10° / min, Scanning angle 2θ: 10–90°. CH crystal, Aft crystal, AFM crystal, C2S, C3S, C3A, and C4AF
Differential Scanning Calorimetry Fewer than 150 μm Dried at 105°C for 4 h, Temperature programmed rate was 15°C / min, Gas flow rate:50 mL/min Weight loss