Table 2.
Reaction conditions: iodide 0.1 mmol, amine 1.7 equiv, CuI 10 mol %, ligand 10 mol %, 100 mg 4 Å MS, HE 1 equiv, K3PO4 4 equiv,DMSO 0.2 M, 90 °C, 24 h.
HE = Hantzsch ester
Reaction conditions: iodide 0.1 mmol, amine 1.7 equiv, CuI 10 mol %, ligand 10 mol %, 100 mg 4 Å MS, HE 1 equiv, K3PO4 4 equiv,DMSO 0.2 M, 90 °C, 24 h.
HE = Hantzsch ester