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a) Molecular structure of [H6bpy‐Yb(hfac)3] (1), b) chemical reaction for the formation of [H6(Py)2Yb(hfac)3] n (2), c) X‐ray structure of M‐2 along the c axis with H6(Py)2 ligand and Yb(hfac)3 moieties respectively drawn in capped sticks and spacefill representations, and d) supramolecular arrangement of the two enantiomers along the a axis.
