Table 2. C–N Coupling Reaction Results Using ChemBeads Prepared by Different Coating Methods.
| coating method | actual loading (w/w) | bead mass (mg) | actual reagent mass (mg) | percent conversion |
|---|---|---|---|---|
| free catalyst | 0.5 | 82 | ||
| RAM | 4.61 | 10 | 0.46 | 89 |
| hand mixing | 3.96 | 10 | 0.39 | 89 |
| vortex mixer | 5.01 | 10 | 0.50 | 85 |
| mini vortex mixer | 4.31 | 10 | 0.43 | 83 |