Table 3.
The underlying reason for the high FAME yield obtained by thermally activating Zn5 at different temperatures.
| Activation temp. (°C) | Phase | Reason for high FAME yields |
|---|---|---|
| ≤80 |
1-phase system Zn5(OH)8(NO3)2 |
The acidity increases as the activation temperature rises. |
| 90–140 |
2-phase system Zn5(OH)8(NO3)2 ZnO |
Sufficiently higher ZnO content resulted in an increase in acidity. |
| 170 |
3-phase system Zn5(OH)8(NO3)2 ZnO Zn3(OH)4(NO3)2 |
Sufficiently higher ZnO content resulted in an increase in acidity. Zn3(OH)4(NO3)2 exhibited no negative effects on the esterification activity. |