Table 1. Refined Lattice Parameters, Cell Volumes, and Refinement Factors for SnS Films Deposited at 375 to 445 °C by Rietveld Refinement.
lattice
parameters (Å) |
|||||||
---|---|---|---|---|---|---|---|
deposition temperature (°C) | a | b | c | cell volume (Å3) | crystallite size (nm) | Rwp | GOF |
375 | 4.3231(3) | 11.2043(7) | 3.9883(3) | 193.18(2) | 170(40) | 6.87 | 1.84 |
397 | 4.3035(4) | 11.2080(11) | 3.9975(3) | 192.81(3) | 150(17) | 7.39 | 1.83 |
418 | 4.3063(3) | 11.2083(12) | 3.9960(3) | 192.87(3) | 116(30) | 9.66 | 2.09 |
445 | 4.3024(4) | 11.2272(11) | 3.9963(4) | 193.01(3) | 100(20) | 9.25 | 1.98 |