TABLE 1.

Compound-specific properties of separation and detection

Compound	Retention time (min)	Charge	Parent peak (m/z)	CIa (%)	Major fragments (m/z)	LODb (ng)	Yieldd (%)
Nivalenol	6.9	−	371.0	10.5	311.0, 280.0	200	7
T2-tetraol	6.1	+	321.1	15.8	291.1, 263.1, 260.0	20	31
DON	10.4	−	265.1	15.0	217.2, 138.2, 247.2c	200	9
Verrucarol	12.6	+	289.1	14.6	245.1, 259.1, 274.0	20	46
3-Ace-DON	13.1	−	337.3	19.0	307.1, 295.2, 277.1	200	10
DAS	14.4	+	389.2	19.0	329.1, 247.2	2	52
Citrinine	14.5	+	251.5	13.5	265.1, 233.2	20	10
T2-triol	14.9	+	405.3	19.0	333.9, 303.1	2	63
Ochratoxin A	15.2	+	426.2	17.2	279.0, 261.1	20	45
Satratoxin G (SATG)	15.9	+	567.2	24.0	523.2, 493.0, 263.1,c, 231.1c	0.2	88
HT2	16.2	+	447.2	17.7	345.1, 387.2,c 285.1	0.2	76
SATH	16.6	+	551.5	25.0	523.1, 507.2,c 321.1,c 303.0c	0.2	39
Verrucarine A	17.6	+	525.2	20.8	497.2, 295.1, 249.1,c 231.2c	0.02	47
T2 toxin	18.1	+	489.1	19.7	387.1, 327.2, 245.1	0.02	82
RDRA	18.2	+	555.2	25.0	527.2, 325.1, 279.1, 231.4c	0.02	92
Acetyl-T2 toxin	22.3	+	531.6	20.3	429.1, 369.4, 287.5	0.02	85
Sterigmatocystin	25.7	+	325.5	18.5	310.1, 297.3	2	67
Reserpine (internal standard)	16.4	+	609.3	24.0	609.3, 448.4, 397.1	0.02	76

^aCI, relative collision intensity. 

^bLOD, limit of detection. 

^cFragment not used for quantitation. 

^dYield of extraction procedure.