Table 2.
No. | 1 | 2 | 3 | 4 | 5 | 6 | 7 |
---|---|---|---|---|---|---|---|
δC d | δC e | δC e | δC d | δC d | δC d | δC d | |
1 | 39.8, C | 39.9, C | 39.8, C | 39.8, C | 40.0, C | 39.5, C | 39.8, C |
2 | 52.7, CH | 52.8, CH | 52.8, CH | 52.6, CH | 52.9, CH | 52.3, CH | 52.1, CH |
3 | 32.8, CH2 | 34.3, CH2 | 34.3, CH2 | 32.4, CH2 | 33.4, CH2 | 32.0, CH2 | 29.5, CH2 |
4 | 42.3, CH | 40.7, CH | 34.72, CH | 49.4, CH | 45.0, CH | 41.2, CH | 49.6, CH |
5 | 26.4, CH2 | 26.7, CH2 | 26.6, CH2 | 26.4, CH2 | 27.4, CH2 | 26.2, CH2 | 24.0, CH2 |
6 | 39.8, CH2 | 39.8, CH2 | 40.0, CH2 | 39.7, CH2 | 40.1, CH2 | 39.7, CH2 | 39.2, CH2 |
7 | 16.8, CH3 | 16.7, CH3 | 16.7, CH3 | 16.8, CH3 | 16.8, CH3 | 16.7, CH3 | 16.6, CH3 |
8 | 150.3, CH | 150.2, CH | 150.3, CH | 149.8, CH | 150.3, CH | 150.0, CH | 149.8, CH |
9 | 110.1, CH2 | 110.1, CH2 | 110.1, CH2 | 110.4, CH2 | 110.1, CH2 | 110.3, CH2 | 110.5, CH2 |
10 | 147.5, C | 147.6, C | 147.5, C | 147.3, C | 147.7, C | 147.3, C | 147.0, C |
11 | 112.4, CH2 | 112.4, CH2 | 112.3, CH2 | 112.6, CH2 | 112.4, CH2 | 112.5, CH2 | 112.9, CH2 |
12 | 24.9, CH3 | 25.0, CH3 | 25.0, CH3 | 25.0, CH3 | 24.9, CH3 | 25.1, CH3 | 24.9, CH3 |
13 | 146.3, C | 137.5, C | 122.9, C | 164.4, C | 153.2, C | 155.5, C | 202.0, C |
14 | 99.2, CH | 101.0, CH | 158.8, CH | 18.5, CH3 | 107.6, CH2 | 21.1, CH3 | 130.7, CH |
15 | 115.7, CH | 124.6, CH | 192.3, C | 122.5, CH | 28.4, CH2 | 124.2, CH | 139.5, CH |
16 | 28.0, CH2 | 25.6, CH2 | 37.3, CH2 | 203.0, C | 34.4, CH2 | 138.2, CH | 79.2, CH |
17 | 80.1, CH | 73.1, CH | 84.8, CH | 54.4, CH2 | 214.1, C | 128.4, CH | 72.3, C |
18 | 81.3, C | 72.3, C | 71.4, C | 70.1, C | 76.4, C | 199.0, C | 26.4, CH3 |
19 | 29.9, CH3 | 26.4, CH3 | 26.0, CH3 | 29.6, CH3 | 26.8, CH3 | 28.3, CH3 | 25.6, CH3 |
20 | 24.0, CH3 | 23.5, CH3 | 24.6, CH3 | 29.6, CH3 | 26.8, CH3 | 170.1, C | |
21 | 21.2, CH3 |
c The assignments were based on HMQC and HMBC spectra. d Spectra recorded at 125 MHz. e Spectra recorded at 150 MHz.