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. 2023 Mar 30;21(4):223. doi: 10.3390/md21040223

Table 2.

13C NMR data of lobocatalens A–G (17) (CDCl3) c.

No. 1 2 3 4 5 6 7
δC d δC e δC e δC d δC d δC d δC d
1 39.8, C 39.9, C 39.8, C 39.8, C 40.0, C 39.5, C 39.8, C
2 52.7, CH 52.8, CH 52.8, CH 52.6, CH 52.9, CH 52.3, CH 52.1, CH
3 32.8, CH2 34.3, CH2 34.3, CH2 32.4, CH2 33.4, CH2 32.0, CH2 29.5, CH2
4 42.3, CH 40.7, CH 34.72, CH 49.4, CH 45.0, CH 41.2, CH 49.6, CH
5 26.4, CH2 26.7, CH2 26.6, CH2 26.4, CH2 27.4, CH2 26.2, CH2 24.0, CH2
6 39.8, CH2 39.8, CH2 40.0, CH2 39.7, CH2 40.1, CH2 39.7, CH2 39.2, CH2
7 16.8, CH3 16.7, CH3 16.7, CH3 16.8, CH3 16.8, CH3 16.7, CH3 16.6, CH3
8 150.3, CH 150.2, CH 150.3, CH 149.8, CH 150.3, CH 150.0, CH 149.8, CH
9 110.1, CH2 110.1, CH2 110.1, CH2 110.4, CH2 110.1, CH2 110.3, CH2 110.5, CH2
10 147.5, C 147.6, C 147.5, C 147.3, C 147.7, C 147.3, C 147.0, C
11 112.4, CH2 112.4, CH2 112.3, CH2 112.6, CH2 112.4, CH2 112.5, CH2 112.9, CH2
12 24.9, CH3 25.0, CH3 25.0, CH3 25.0, CH3 24.9, CH3 25.1, CH3 24.9, CH3
13 146.3, C 137.5, C 122.9, C 164.4, C 153.2, C 155.5, C 202.0, C
14 99.2, CH 101.0, CH 158.8, CH 18.5, CH3 107.6, CH2 21.1, CH3 130.7, CH
15 115.7, CH 124.6, CH 192.3, C 122.5, CH 28.4, CH2 124.2, CH 139.5, CH
16 28.0, CH2 25.6, CH2 37.3, CH2 203.0, C 34.4, CH2 138.2, CH 79.2, CH
17 80.1, CH 73.1, CH 84.8, CH 54.4, CH2 214.1, C 128.4, CH 72.3, C
18 81.3, C 72.3, C 71.4, C 70.1, C 76.4, C 199.0, C 26.4, CH3
19 29.9, CH3 26.4, CH3 26.0, CH3 29.6, CH3 26.8, CH3 28.3, CH3 25.6, CH3
20 24.0, CH3 23.5, CH3 24.6, CH3 29.6, CH3 26.8, CH3 170.1, C
21 21.2, CH3

c The assignments were based on HMQC and HMBC spectra. d Spectra recorded at 125 MHz. e Spectra recorded at 150 MHz.