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. 2023 Apr 25;8(Pt 4):x230355. doi: 10.1107/S2414314623003553
Rh1—As 2.3337 (4) C6—C5 1.379 (4)
Rh1—O2 2.0682 (17) C28—H28 0.9500
Rh1—O1 2.0338 (18) C28—C29 1.376 (4)
Rh1—C02 1.813 (3) C9—H9 0.9500
As—C26 1.933 (2) C9—C10 1.395 (4)
As—C14 1.932 (2) C3—H3 0.9500
As—C20 1.939 (2) C3—C4 1.386 (4)
O2—C1 1.301 (3) C18—H18 0.9500
O1—N1 1.367 (3) C18—C17 1.387 (4)
O02—C02 1.144 (3) C11—H11 0.9500
N1—C1 1.319 (3) C11—C12 1.387 (4)
N1—C8 1.437 (3) C11—C10 1.375 (4)
C1—C2 1.479 (3) C31—H31 0.9500
C26—C27 1.388 (4) C31—C30 1.384 (4)
C26—C31 1.392 (4) C12—H12 0.9500
C8—C13 1.387 (4) C16—H16 0.9500
C8—C9 1.385 (4) C16—C17 1.381 (4)
C14—C15 1.395 (3) C4—H4 0.9500
C14—C19 1.393 (3) C4—C5 1.391 (4)
C20—C25 1.371 (4) C10—H10 0.9500
C20—C21 1.384 (4) C17—H17 0.9500
C15—H15 0.9500 C5—H5 0.9500
C15—C16 1.388 (4) C29—H29 0.9500
C7—H7 0.9500 C29—C30 1.385 (4)
C7—C2 1.397 (4) C25—H25 0.9500
C7—C6 1.391 (4) C25—C24 1.390 (4)
C27—H27 0.9500 C24—H24 0.9500
C27—C28 1.395 (4) C24—C23 1.371 (5)
C13—H13 0.9500 C21—H21 0.9500
C13—C12 1.385 (4) C21—C22 1.391 (4)
C2—C3 1.389 (4) C23—H23 0.9500
C19—H19 0.9500 C23—C22 1.374 (5)
C19—C18 1.390 (4) C30—H30 0.9500
C6—H6 0.9500 C22—H22 0.9500
O2—Rh1—As 171.06 (5) C29—C28—H28 119.8
O1—Rh1—As 91.66 (5) C8—C9—H9 120.6
O1—Rh1—O2 79.53 (7) C8—C9—C10 118.8 (2)
C02—Rh1—As 89.53 (8) C10—C9—H9 120.6
C02—Rh1—O2 99.31 (9) C2—C3—H3 119.9
C02—Rh1—O1 178.39 (10) C4—C3—C2 120.2 (3)
C26—As—Rh1 118.78 (7) C4—C3—H3 119.9
C26—As—C20 103.15 (10) C19—C18—H18 120.1
C14—As—Rh1 112.68 (7) C17—C18—C19 119.7 (3)
C14—As—C26 104.81 (11) C17—C18—H18 120.1
C14—As—C20 100.97 (11) C12—C11—H11 119.7
C20—As—Rh1 114.44 (8) C10—C11—H11 119.7
C1—O2—Rh1 111.54 (15) C10—C11—C12 120.6 (3)
N1—O1—Rh1 110.33 (13) C26—C31—H31 119.9
O1—N1—C8 114.38 (19) C30—C31—C26 120.3 (3)
C1—N1—O1 119.1 (2) C30—C31—H31 119.9
C1—N1—C8 126.2 (2) C13—C12—C11 119.9 (3)
O2—C1—N1 119.3 (2) C13—C12—H12 120.0
O2—C1—C2 117.1 (2) C11—C12—H12 120.0
N1—C1—C2 123.5 (2) C15—C16—H16 120.1
C27—C26—As 122.12 (19) C17—C16—C15 119.8 (3)
C27—C26—C31 119.6 (2) C17—C16—H16 120.1
C31—C26—As 118.27 (19) C3—C4—H4 119.9
C13—C8—N1 118.2 (2) C3—C4—C5 120.2 (3)
C9—C8—N1 120.5 (2) C5—C4—H4 119.9
C9—C8—C13 121.3 (2) C9—C10—H10 119.9
C15—C14—As 121.74 (19) C11—C10—C9 120.1 (3)
C19—C14—As 118.28 (19) C11—C10—H10 119.9
C19—C14—C15 119.9 (2) C18—C17—H17 119.6
C25—C20—As 118.6 (2) C16—C17—C18 120.7 (3)
C25—C20—C21 118.7 (3) C16—C17—H17 119.6
C21—C20—As 122.7 (2) C6—C5—C4 119.7 (2)
C14—C15—H15 120.1 C6—C5—H5 120.1
C16—C15—C14 119.9 (2) C4—C5—H5 120.1
C16—C15—H15 120.1 C28—C29—H29 120.0
C2—C7—H7 120.2 C28—C29—C30 120.1 (3)
C6—C7—H7 120.2 C30—C29—H29 120.0
C6—C7—C2 119.5 (2) C20—C25—H25 119.5
C26—C27—H27 120.2 C20—C25—C24 121.0 (3)
C26—C27—C28 119.7 (3) C24—C25—H25 119.5
C28—C27—H27 120.2 C25—C24—H24 120.0
C8—C13—H13 120.4 C23—C24—C25 120.0 (3)
C12—C13—C8 119.1 (3) C23—C24—H24 120.0
C12—C13—H13 120.4 C20—C21—H21 119.9
C7—C2—C1 123.2 (2) C20—C21—C22 120.3 (3)
C3—C2—C1 117.0 (2) C22—C21—H21 119.9
C3—C2—C7 119.7 (2) C24—C23—H23 120.3
C14—C19—H19 120.1 C24—C23—C22 119.5 (3)
C18—C19—C14 119.8 (2) C22—C23—H23 120.3
C18—C19—H19 120.1 C31—C30—C29 120.0 (3)
O02—C02—Rh1 178.5 (2) C31—C30—H30 120.0
C7—C6—H6 119.7 C29—C30—H30 120.0
C5—C6—C7 120.7 (3) C21—C22—H22 119.8
C5—C6—H6 119.7 C23—C22—C21 120.3 (3)
C27—C28—H28 119.8 C23—C22—H22 119.8
C29—C28—C27 120.4 (3)
Rh1—O2—C1—N1 4.4 (3) C8—C9—C10—C11 1.5 (4)
Rh1—O2—C1—C2 −177.62 (16) C14—C15—C16—C17 −0.4 (4)
Rh1—O1—N1—C1 1.5 (3) C14—C19—C18—C17 −0.2 (4)
Rh1—O1—N1—C8 175.94 (16) C20—C25—C24—C23 −1.8 (6)
As—C26—C27—C28 −178.1 (2) C20—C21—C22—C23 −1.2 (5)
As—C26—C31—C30 179.1 (2) C15—C14—C19—C18 −1.6 (4)
As—C14—C15—C16 −175.2 (2) C15—C16—C17—C18 −1.4 (4)
As—C14—C19—C18 175.6 (2) C7—C2—C3—C4 0.4 (4)
As—C20—C25—C24 −176.8 (3) C7—C6—C5—C4 −0.1 (4)
As—C20—C21—C22 178.4 (3) C27—C26—C31—C30 1.4 (4)
O2—C1—C2—C7 137.2 (2) C27—C28—C29—C30 0.6 (5)
O2—C1—C2—C3 −39.0 (3) C13—C8—C9—C10 −4.1 (4)
O1—N1—C1—O2 −4.1 (3) C2—C7—C6—C5 −0.8 (4)
O1—N1—C1—C2 178.1 (2) C2—C3—C4—C5 −1.3 (4)
O1—N1—C8—C13 −58.9 (3) C19—C14—C15—C16 1.9 (4)
O1—N1—C8—C9 121.5 (2) C19—C18—C17—C16 1.7 (4)
N1—C1—C2—C7 −45.0 (4) C6—C7—C2—C1 −175.5 (2)
N1—C1—C2—C3 138.8 (3) C6—C7—C2—C3 0.6 (4)
N1—C8—C13—C12 −175.6 (2) C28—C29—C30—C31 0.3 (5)
N1—C8—C9—C10 175.5 (2) C9—C8—C13—C12 4.0 (4)
C1—N1—C8—C13 115.1 (3) C3—C4—C5—C6 1.1 (4)
C1—N1—C8—C9 −64.5 (3) C31—C26—C27—C28 −0.5 (4)
C1—C2—C3—C4 176.7 (2) C12—C11—C10—C9 1.2 (4)
C26—C27—C28—C29 −0.5 (4) C10—C11—C12—C13 −1.3 (4)
C26—C31—C30—C29 −1.3 (5) C25—C20—C21—C22 −3.2 (5)
C8—N1—C1—O2 −177.9 (2) C25—C24—C23—C22 −2.7 (5)
C8—N1—C1—C2 4.3 (4) C24—C23—C22—C21 4.2 (5)
C8—C13—C12—C11 −1.3 (4) C21—C20—C25—C24 4.7 (5)