Ge1—C1 | 1.9331 (13) | Ge2—C17 | 1.9370 (13) |
Ge1—C5 | 1.9326 (14) | Ge2—C21 | 1.9290 (13) |
Ge1—C9 | 1.9299 (14) | Ge2—C25 | 1.9329 (13) |
Ge1—C13 | 1.9351 (14) | Ge2—C29 | 1.9353 (14) |
O1—C1 | 1.3776 (17) | O5—C17 | 1.3806 (16) |
O1—C4 | 1.4592 (19) | O5—C20 | 1.4641 (19) |
O2—C5 | 1.3852 (17) | O6—C21 | 1.3816 (17) |
O2—C8 | 1.4649 (17) | O6—C24 | 1.4624 (19) |
O3—C9 | 1.3797 (17) | O7—C25 | 1.3877 (16) |
O3—C12 | 1.4595 (18) | O7—C28 | 1.4619 (16) |
O4—C13 | 1.3822 (16) | O8—C29 | 1.3840 (17) |
O4—C16 | 1.4603 (19) | O8—C32 | 1.4592 (17) |
C1—C2 | 1.323 (2) | C17—C18 | 1.3314 (19) |
C2—H2 | 0.95 (2) | C18—H18 | 0.97 (2) |
C2—C3 | 1.501 (2) | C18—C19 | 1.505 (2) |
C3—H3A | 0.93 (2) | C19—H19A | 0.99 (2) |
C3—H3B | 0.97 (2) | C19—H19B | 1.02 (2) |
C3—C4 | 1.518 (2) | C19—C20 | 1.526 (2) |
C4—H4A | 0.93 (2) | C20—H20A | 0.952 (18) |
C4—H4B | 1.02 (2) | C20—H20B | 0.97 (2) |
C5—C6 | 1.331 (2) | C21—C22 | 1.326 (2) |
C6—H6 | 0.97 (2) | C22—H22 | 0.93 (2) |
C6—C7 | 1.511 (2) | C22—C23 | 1.503 (2) |
C7—C8 | 1.528 (2) | C23—C24 | 1.529 (2) |
C7—H7A | 0.96 (2) | C23—H23A | 0.97 (2) |
C7—H7B | 1.05 (2) | C23—H23B | 0.97 (2) |
C8—H8A | 1.00 (2) | C24—H24A | 0.97 (2) |
C8—H8B | 0.899 (18) | C24—H24B | 0.97 (2) |
C9—C10 | 1.325 (2) | C25—C26 | 1.3313 (19) |
C10—H10 | 0.98 (2) | C26—H26 | 0.96 (2) |
C10—C11 | 1.509 (3) | C26—C27 | 1.5119 (19) |
C11—H11A | 1.04 (2) | C27—H27A | 0.95 (2) |
C11—H11B | 0.960 (19) | C27—H27B | 1.00 (2) |
C11—C12 | 1.530 (3) | C27—C28 | 1.531 (2) |
C12—H12A | 0.94 (2) | C28—H28A | 0.946 (19) |
C12—H12B | 0.951 (19) | C28—H28B | 0.930 (18) |
C13—C14 | 1.328 (2) | C29—C30 | 1.3266 (19) |
C14—H14 | 0.92 (2) | C30—H30 | 0.974 (19) |
C14—C15 | 1.503 (2) | C30—C31 | 1.506 (2) |
C15—H15A | 0.97 (2) | C31—H31A | 0.964 (19) |
C15—H15B | 1.046 (19) | C31—H31B | 0.98 (2) |
C15—C16 | 1.532 (2) | C31—C32 | 1.529 (2) |
C16—H16A | 0.96 (2) | C32—H32A | 0.96 (2) |
C16—H16B | 0.950 (18) | C32—H32B | 0.920 (19) |
C1—Ge1—C13 | 109.37 (6) | C21—Ge2—C17 | 108.03 (6) |
C5—Ge1—C1 | 109.74 (6) | C21—Ge2—C25 | 108.58 (5) |
C5—Ge1—C13 | 108.78 (6) | C21—Ge2—C29 | 112.88 (6) |
C9—Ge1—C1 | 107.67 (6) | C25—Ge2—C17 | 107.92 (5) |
C9—Ge1—C5 | 108.46 (6) | C25—Ge2—C29 | 106.91 (6) |
C9—Ge1—C13 | 112.79 (6) | C29—Ge2—C17 | 112.36 (6) |
C1—O1—C4 | 107.12 (11) | C17—O5—C20 | 106.95 (11) |
C5—O2—C8 | 106.84 (11) | C21—O6—C24 | 107.04 (12) |
C9—O3—C12 | 106.83 (12) | C25—O7—C28 | 106.57 (10) |
C13—O4—C16 | 107.29 (11) | C29—O8—C32 | 107.01 (11) |
O1—C1—Ge1 | 115.90 (10) | O5—C17—Ge2 | 118.30 (9) |
C2—C1—Ge1 | 130.51 (11) | C18—C17—Ge2 | 128.10 (11) |
C2—C1—O1 | 113.56 (13) | C18—C17—O5 | 113.59 (12) |
C1—C2—H2 | 124.1 (12) | C17—C18—H18 | 125.9 (12) |
C1—C2—C3 | 110.22 (13) | C17—C18—C19 | 110.14 (13) |
C3—C2—H2 | 125.5 (12) | C19—C18—H18 | 123.9 (12) |
C2—C3—H3A | 112.3 (13) | C18—C19—H19A | 110.0 (11) |
C2—C3—H3B | 113.2 (12) | C18—C19—H19B | 110.1 (11) |
C2—C3—C4 | 101.79 (13) | C18—C19—C20 | 101.56 (12) |
H3A—C3—H3B | 106.4 (17) | H19A—C19—H19B | 113.0 (16) |
C4—C3—H3A | 111.9 (14) | C20—C19—H19A | 111.0 (12) |
C4—C3—H3B | 111.4 (13) | C20—C19—H19B | 110.7 (11) |
O1—C4—C3 | 107.18 (12) | O5—C20—C19 | 107.20 (12) |
O1—C4—H4A | 109.2 (13) | O5—C20—H20A | 107.9 (11) |
O1—C4—H4B | 106.5 (13) | O5—C20—H20B | 106.7 (12) |
C3—C4—H4A | 111.6 (13) | C19—C20—H20A | 110.3 (11) |
C3—C4—H4B | 111.0 (13) | C19—C20—H20B | 111.1 (12) |
H4A—C4—H4B | 111.1 (18) | H20A—C20—H20B | 113.3 (16) |
O2—C5—Ge1 | 117.07 (10) | O6—C21—Ge2 | 116.77 (10) |
C6—C5—Ge1 | 129.06 (12) | C22—C21—Ge2 | 129.17 (11) |
C6—C5—O2 | 113.85 (13) | C22—C21—O6 | 113.68 (13) |
C5—C6—H6 | 127.5 (12) | C21—C22—H22 | 123.3 (13) |
C5—C6—C7 | 109.74 (14) | C21—C22—C23 | 110.38 (13) |
C7—C6—H6 | 122.8 (12) | C23—C22—H22 | 126.3 (12) |
C6—C7—C8 | 101.79 (12) | C22—C23—C24 | 101.63 (12) |
C6—C7—H7A | 114.6 (13) | C22—C23—H23A | 114.8 (13) |
C6—C7—H7B | 107.8 (12) | C22—C23—H23B | 114.0 (13) |
C8—C7—H7A | 112.0 (13) | C24—C23—H23A | 111.5 (13) |
C8—C7—H7B | 112.1 (12) | C24—C23—H23B | 108.5 (14) |
H7A—C7—H7B | 108.5 (17) | H23A—C23—H23B | 106.3 (17) |
O2—C8—C7 | 107.01 (12) | O6—C24—C23 | 107.24 (13) |
O2—C8—H8A | 107.6 (12) | O6—C24—H24A | 106.5 (13) |
O2—C8—H8B | 103.9 (11) | O6—C24—H24B | 107.8 (13) |
C7—C8—H8A | 115.4 (12) | C23—C24—H24A | 111.3 (13) |
C7—C8—H8B | 114.0 (11) | C23—C24—H24B | 112.0 (14) |
H8A—C8—H8B | 108.1 (16) | H24A—C24—H24B | 111.7 (18) |
O3—C9—Ge1 | 118.25 (9) | O7—C25—Ge2 | 116.20 (9) |
C10—C9—Ge1 | 127.58 (12) | C26—C25—Ge2 | 130.20 (11) |
C10—C9—O3 | 114.16 (14) | C26—C25—O7 | 113.59 (12) |
C9—C10—H10 | 127.0 (13) | C25—C26—H26 | 128.1 (12) |
C9—C10—C11 | 109.94 (15) | C25—C26—C27 | 109.57 (13) |
C11—C10—H10 | 123.1 (13) | C27—C26—H26 | 122.3 (12) |
C10—C11—H11A | 111.0 (12) | C26—C27—H27A | 113.8 (12) |
C10—C11—H11B | 109.9 (12) | C26—C27—H27B | 108.9 (11) |
C10—C11—C12 | 101.51 (13) | C26—C27—C28 | 101.32 (11) |
H11A—C11—H11B | 109.4 (16) | H27A—C27—H27B | 108.9 (16) |
C12—C11—H11A | 111.8 (11) | C28—C27—H27A | 110.9 (12) |
C12—C11—H11B | 113.0 (12) | C28—C27—H27B | 113.0 (11) |
O3—C12—C11 | 107.40 (13) | O7—C28—C27 | 106.50 (11) |
O3—C12—H12A | 107.2 (12) | O7—C28—H28A | 108.0 (12) |
O3—C12—H12B | 105.2 (12) | O7—C28—H28B | 104.8 (11) |
C11—C12—H12A | 114.5 (12) | C27—C28—H28A | 116.2 (12) |
C11—C12—H12B | 112.1 (12) | C27—C28—H28B | 113.2 (11) |
H12A—C12—H12B | 110.0 (16) | H28A—C28—H28B | 107.4 (16) |
O4—C13—Ge1 | 117.16 (10) | O8—C29—Ge2 | 114.61 (9) |
C14—C13—Ge1 | 129.45 (11) | C30—C29—Ge2 | 131.68 (11) |
C14—C13—O4 | 113.39 (13) | C30—C29—O8 | 113.71 (12) |
C13—C14—H14 | 123.4 (13) | C29—C30—H30 | 125.3 (12) |
C13—C14—C15 | 110.38 (13) | C29—C30—C31 | 109.97 (13) |
C15—C14—H14 | 126.2 (13) | C31—C30—H30 | 124.8 (12) |
C14—C15—H15A | 111.2 (11) | C30—C31—H31A | 107.8 (12) |
C14—C15—H15B | 111.5 (11) | C30—C31—H31B | 110.4 (13) |
C14—C15—C16 | 101.60 (12) | C30—C31—C32 | 101.74 (12) |
H15A—C15—H15B | 109.1 (15) | H31A—C31—H31B | 112.5 (17) |
C16—C15—H15A | 112.0 (12) | C32—C31—H31A | 112.3 (11) |
C16—C15—H15B | 111.2 (11) | C32—C31—H31B | 111.5 (13) |
O4—C16—C15 | 106.89 (12) | O8—C32—C31 | 106.96 (12) |
O4—C16—H16A | 108.0 (12) | O8—C32—H32A | 106.6 (13) |
O4—C16—H16B | 108.1 (11) | O8—C32—H32B | 107.1 (12) |
C15—C16—H16A | 110.4 (12) | C31—C32—H32A | 114.2 (12) |
C15—C16—H16B | 113.0 (11) | C31—C32—H32B | 111.4 (11) |
H16A—C16—H16B | 110.2 (16) | H32A—C32—H32B | 110.2 (16) |
Ge1—C1—C2—C3 | 176.36 (12) | Ge2—C17—C18—C19 | 176.68 (11) |
Ge1—C5—C6—C7 | 178.01 (11) | Ge2—C21—C22—C23 | −170.77 (12) |
Ge1—C9—C10—C11 | 179.83 (11) | Ge2—C25—C26—C27 | −178.47 (10) |
Ge1—C13—C14—C15 | −179.37 (11) | Ge2—C29—C30—C31 | −178.54 (11) |
O1—C1—C2—C3 | −1.5 (2) | O5—C17—C18—C19 | −1.66 (19) |
O2—C5—C6—C7 | −0.57 (18) | O6—C21—C22—C23 | 1.84 (19) |
O3—C9—C10—C11 | −0.27 (19) | O7—C25—C26—C27 | 1.18 (17) |
O4—C13—C14—C15 | 0.09 (19) | O8—C29—C30—C31 | 0.67 (18) |
C1—O1—C4—C3 | 2.7 (2) | C17—O5—C20—C19 | 6.77 (18) |
C1—C2—C3—C4 | 3.0 (2) | C17—C18—C19—C20 | 5.58 (19) |
C2—C3—C4—O1 | −3.4 (2) | C18—C19—C20—O5 | −7.30 (18) |
C4—O1—C1—Ge1 | −179.00 (13) | C20—O5—C17—Ge2 | 178.16 (10) |
C4—O1—C1—C2 | −0.8 (2) | C20—O5—C17—C18 | −3.32 (18) |
C5—O2—C8—C7 | 8.45 (15) | C21—O6—C24—C23 | 0.6 (2) |
C5—C6—C7—C8 | 5.62 (17) | C21—C22—C23—C24 | −1.27 (19) |
C6—C7—C8—O2 | −8.37 (16) | C22—C23—C24—O6 | 0.35 (19) |
C8—O2—C5—Ge1 | 176.14 (9) | C24—O6—C21—Ge2 | 172.03 (11) |
C8—O2—C5—C6 | −5.10 (16) | C24—O6—C21—C22 | −1.55 (19) |
C9—O3—C12—C11 | −4.04 (16) | C25—O7—C28—C27 | −15.01 (14) |
C9—C10—C11—C12 | −2.19 (18) | C25—C26—C27—C28 | −10.12 (16) |
C10—C11—C12—O3 | 3.72 (17) | C26—C27—C28—O7 | 14.94 (14) |
C12—O3—C9—Ge1 | −177.31 (10) | C28—O7—C25—Ge2 | −171.34 (9) |
C12—O3—C9—C10 | 2.78 (18) | C28—O7—C25—C26 | 8.96 (16) |
C13—O4—C16—C15 | 6.62 (18) | C29—O8—C32—C31 | 7.81 (15) |
C13—C14—C15—C16 | 3.90 (18) | C29—C30—C31—C32 | 4.11 (17) |
C14—C15—C16—O4 | −6.24 (17) | C30—C31—C32—O8 | −7.10 (16) |
C16—O4—C13—Ge1 | 175.18 (11) | C32—O8—C29—Ge2 | 173.88 (9) |
C16—O4—C13—C14 | −4.35 (19) | C32—O8—C29—C30 | −5.48 (17) |