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. 2022 Oct 26;88(10):6420–6433. doi: 10.1021/acs.joc.2c01963

Table 2. Scope of the Reactiona.

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a

Standard reaction conditions: (a) 1 (0.20 mmol), K2CO3 (0.20 equiv, 0.04 mmol), NCS (3.0 equiv, 0.60 mmol), [Ru(bpy)3](PF6)2 (5 mol %, 0.01 mmol), anhydrous PhCH3 (3 mL), anhydrous HCO2CH3 (1 mL), N2 atmosphere irradiation with 456 nm light source for 21 h, blue light. (b) Yields determined on isolated products. (c) Reaction scaled up to 1 mmol, 36 h reaction time. (d) 36 h reaction time.