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. 2023 May 24;257:115487. doi: 10.1016/j.ejmech.2023.115487

Scheme 3.

Scheme 3

Synthesis of compounds A7, A13, A15, A17, A20, B1B17. Reagents and conditions: (a) I2, EtOH, reflux, 3–5 h, 40%–80%; (b) BBr3/DCM, DCM, −10 °C to rt, 24–36 h, 40%–63%.