Table 1. Crystallographic statistics.
Data collection | |
---|---|
Resolution range (Å) | 92.38–3.50 (3.56–3.50) |
Space group | P4 22 12 |
Unit cell: a, b, c (Å) | 184.76, 184.76, 105.40 |
Unique reflections | 23570 (1159) |
Multiplicity | 26.8 (28.3) |
Completeness (%) | 100.0 (100.0) |
Mean I/σ( I) | 7.1 (0.5) |
CC 1/2 | 0.997 (0.424) |
R pim | 0.073 (0.871) |
Refinement | |
Non-hydrogen atoms
Protein Glycan Ion |
9992 333 1 Ni 2+, 1 Cl - |
R work/ R free | 0.265/0.319 |
Root-mean-square deviations
Bonds (Å) Angles (°) |
0.004 0.638 |
Ramachandran plot
Favoured (%) Allowed (%) Outliers (%) |
90.1 9.2 0.7 |