Table 4.
Comparison of the catalytic efficiency of Cs/ECH-TMA solid acid (1) with other heterogeneous or homogeneous catalysts for the synthesis of 6a.
| Entry | Catalyst | Catalyst loading | Solvent | Temp. oC | Time (min) | Yield (%) | Ref. |
|---|---|---|---|---|---|---|---|
| 1 | Co3O4-CNTs | 30 mg | EtOH | Reflux | 35 | 97 | [114] |
| 2 | Vitamin-B1 | 20 mol% | EtOH | Reflux | 60 | 90 | [115] |
| 3 | Fe(HSO4)3/SiO2 | 10 mol% | EtOH | 80 | 60 | 95 | [116] |
| 4 | FeF3 | 5 mol% | EtOH | Reflux | 60 | 92 | [117] |
| 5 | Al2(SO4)3 | 10 mol% | EtOH | Reflux | 300 | 87 | [118] |
| 6 | Cs/ECH-TMA | 10 mg | EtOH | Reflux | 35 | 96 | This Work |