1H (400 MHz) and 13C (100 MHz) data of compound 1 in CDCl3 (δ in ppm, J in Hz).
Position | δ C, type | δ H (J in Hz) |
---|---|---|
1 | 68.2, CH2 | 5.14, s |
2 | ||
3 | 169.7, C | |
4 | 108.3, C | |
5 | 155.3, C | |
6 | 115.9, C | |
7 | 157.1, C | |
8 | 114.3, C | |
9 | 145.5, C | |
10 | ||
11 | 79.2, C | |
12 | 44.5, CH2 | 2.64, d (14.5) |
2.39, d (14.5) | ||
13 | 102.0, C | |
14 | 92.2, C | |
15 | 86.7, C | |
16 | ||
17 | 118.5, C | |
18 | 69.2, CH | 3.80, dd (5.5, 0.9) |
19 | 37.7, CH2 | 2.15, dd (15.9, 0.9) |
1.85, dd (15.9, 5.5) | ||
20 | 39.2, C | |
21 | 38.2, CH | 3.05, dd (7.5, 1.8) |
22 | 17.8, CH2 | 2.95, m |
23 | 10.9, CH3 | 2.06, s |
24 | 27.3, CH3 | 1.35, s |
25 | 78.2, CH2 | 4.16, d (9.7) |
3.95, d (9.7) | ||
26 | 23.0, CH3 | 1.69, s |
27 | 19.6, CH3 | 0.87, s |
28 | 49.1, CH3 | 3.53, s |
29 | 62.2, CH3 | 4.16, s |