Skip to main content
. 2023 Jun 1;13(24):16480–16487. doi: 10.1039/d3ra02632a

1H (400 MHz) and 13C (100 MHz) data of compound 1 in CDCl3 (δ in ppm, J in Hz).

Position δ C, type δ H (J in Hz)
1 68.2, CH2 5.14, s
2
3 169.7, C
4 108.3, C
5 155.3, C
6 115.9, C
7 157.1, C
8 114.3, C
9 145.5, C
10
11 79.2, C
12 44.5, CH2 2.64, d (14.5)
2.39, d (14.5)
13 102.0, C
14 92.2, C
15 86.7, C
16
17 118.5, C
18 69.2, CH 3.80, dd (5.5, 0.9)
19 37.7, CH2 2.15, dd (15.9, 0.9)
1.85, dd (15.9, 5.5)
20 39.2, C
21 38.2, CH 3.05, dd (7.5, 1.8)
22 17.8, CH2 2.95, m
23 10.9, CH3 2.06, s
24 27.3, CH3 1.35, s
25 78.2, CH2 4.16, d (9.7)
3.95, d (9.7)
26 23.0, CH3 1.69, s
27 19.6, CH3 0.87, s
28 49.1, CH3 3.53, s
29 62.2, CH3 4.16, s