Table 1.
Analytical curve, coefficient of determination (R2), LOD, LOQ of imidacloprid in solvent and matrix.
Matrix | Parameter | Solvent standard |
Brinjal matrix standard |
||||||
---|---|---|---|---|---|---|---|---|---|
tcal | tcrit | T test | tcal | tcrit | T test | ||||
Brinjal | Analytical curve | Y = 4500.8x-22339 | 2.515 | 2.306 | S | Y = 5322.8x-20619 | 2.421 | 2.306 | S |
R2 | 0.998 | 0.999 | |||||||
LOD | 0.001 μg mL−1 | 0.001 μg/g | |||||||
LOQ | 0.003 μg mL−1 | 0.003 μg/g | |||||||
Matrix effect | 18.26 | ||||||||
Okra | Analytical curve | Y = 774.9x-812.53 | 3.087 | 2.262 | S* | Y = 841.1x-404.28 | 2.841 | 2.262 | S* |
R2* | 0.998 | 0.999 | |||||||
LOD* | 0.001 μg mL−1 | 0.0025 μg/g | |||||||
LOQ* | 0.002 μg mL−1 | 0.008 μg/g | |||||||
Matrix effect | 8.54 |
R2- Coefficient of determination, LOD-Limit of detection, LOQ-Limit of quantification S-significant tcal-t student calculated, tcrit-t student critical.