Table 1. Experimental X-ray Parameters Used for the Two Experiments, Including the Proposal Number, Photon Energy, Beam Size, Flux, Sample Environment, Detector, and Sample–Detector Distance (SDD) for SAXS and WAXS Geometries.

experiment	I-20200072 EC	I-20220280 EC
energy (keV)	12.4	9.0
beam size (μm2)	30 × 30	30 × 30
flux (×109 ph/s)	4.0	6.0
sample environment	Linkam stage	cryostat
SAXS detector	Eiger 500k	Eiger 4M
SAXS SDD (m)	21.2	21.2
WAXS detector	Pilatus 300k	Pilatus 300k
WAXS SDD (m)	0.21	0.20