| Bruker SMART APEXII area detector diffractometer | 4126 independent reflections |
| Radiation source: Micro Focus Rotating Anode, Bruker TXS | 3430 reflections with I > 2σ(I) |
| Double Bounce Multilayer Mirrors monochromator | Rint = 0.082 |
| Detector resolution: 7.407 pixels mm-1 | θmax = 26.4°, θmin = 2.6° |
| ω and φ scans | h = −15→15 |
| Absorption correction: multi-scan (SADABS; Krause et al., 2015) | k = −19→19 |
| Tmin = 0.666, Tmax = 0.744 | l = −14→14 |
| 59713 measured reflections |