Table 2. Experimental details.
| Crystal data | |
| Chemical formula | 2C17H17N4 +·2C7H5O5 −·C17H16N4 |
| M r | 1169.25 |
| Crystal system, space group | Monoclinic, I2/a |
| Temperature (K) | 295 |
| a, b, c (Å) | 16.82625 (15), 16.73298 (17), 26.7833 (3) |
| β (°) | 105.2162 (11) |
| V (Å3) | 7276.57 (14) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.07 |
| Crystal size (mm) | 0.60 × 0.48 × 0.37 |
| Data collection | |
| Diffractometer | Xcalibur, Atlas, Gemini |
| Absorption correction | Gaussian (CrysAlis PRO; Rigaku OD, 2022 ▸) |
| T min, T max | 0.761, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 188774, 11088, 8064 |
| R int | 0.064 |
| (sin θ/λ)max (Å−1) | 0.714 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.049, 0.149, 1.06 |
| No. of reflections | 11088 |
| No. of parameters | 414 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.30, −0.18 |