表3.
不同加标水平下13种HBQs的回收率和精密度(n=6)
Compound | 10 ng/L | 20 ng/L | 50 ng/L | |||||
---|---|---|---|---|---|---|---|---|
Recovery/% | RSD/% | Recovery/% | RSD/% | Recovery/% | RSD/% | |||
2,5-DCBQ | 77 | 4.8 | 75 | 3.7 | 73 | 7.1 | ||
2,6-DCBQ | 85 | 3.0 | 87 | 4.8 | 81 | 3.6 | ||
2,5-DBBQ | 85 | 4.8 | 83 | 2.7 | 80 | 1.9 | ||
2,6-DBBQ | 87 | 4.2 | 82 | 4.0 | 85 | 2.6 | ||
DCMBQ | 86 | 3.5 | 87 | 3.9 | 81 | 4.9 | ||
TriCBQ | 83 | 2.8 | 84 | 3.4 | 78 | 5.7 | ||
2,6-DIBQ | 78 | 7.0 | 81 | 5.4 | 77 | 3.7 | ||
TCBQ | 80 | 3.7 | 84 | 3.0 | 79 | 2.6 | ||
2,6-DBDMBQ | 85 | 3.3 | 88 | 2.3 | 84 | 4.4 | ||
2,3-DBDMBQ | 84 | 1.9 | 85 | 3.7 | 85 | 1.9 | ||
TBBQ | 82 | 3.3 | 77 | 6.2 | 75 | 4.6 | ||
TC-1,2-BQ | 83 | 5.4 | 78 | 6.3 | 76 | 8.3 | ||
TB-1,2-BQ | 66 | 6.6 | 61 | 7.4 | 56 | 9.2 |