Table 2. 13C NMR Spectroscopic Data of 1–4 and Argentatin C (11).
| position | 1 | 2 | 3 | 4 | 11 |
|---|---|---|---|---|---|
| 1 | 33.5 CH2 | 33.3 CH2 | 35.8 CH2 | 33.4 CH2 | 33.3 CH2 |
| 2 | 37.5 CH2 | 37.5 CH2 | 34.6 CH2 | 37.5 CH2 | 37.4 CH2 |
| 3 | 216.6 C | 216.5 C | 217.7 C | 216.6 C | 216.6 C |
| 4 | 50.2 | 50.2 C | 47.4 C | 50.2 C | 50.2 C |
| 5 | 48.5 CH | 48.5 CH | 51.2 CH | 48.5 CH | 48.4 CH |
| 6 | 21.4 CH2 | 21.4 CH2 | 19.3 CH2 | 21.4 CH2 | 21.4 CH2 |
| 7 | 26.1 CH2 | 25.9 CH2 | 26.2 CH2 | 25.9 CH2 | 25.9 CH2 |
| 8 | 47.9 CH | 47.5 CH | 134.3 C | 47.6 CH | 47.5 CH |
| 9 | 20.8 C | 20.6 C | 133.3 C | 20.9 C | 20.8 C |
| 10 | 25.9 C | 26.2 C | 36.9 C | 26.1 C | 25.9 C |
| 11 | 26.4 CH2 | 26.5 CH2 | 20.8 CH2 | 26.4 CH2 | 26.0 CH2 |
| 12 | 32.7 CH2 | 33.5 CH2 | 31.9 CH2* | 32.6 CH2 | 32.5 CH2 |
| 13 | 45.3 C | 46.2 C | 45.3 C* | 45.3 C | 45.3 C |
| 14 | 46.5 C | 46.3 C | 47.2 C* | 46.8 C | 46.6 C |
| 15 | 47.9 CH2 | 48.4 CH2 | 43.9 CH2 | 47.7 CH2 | 47.8 CH2 |
| 16 | 72.4 CH | 73.8 CH | 74.1 CH | 72.8 CH | 72.7 CH |
| 17 | 57.1 CH | 58.6 CH | 57.1 CH | 57.0 CH | 56.7 CH |
| 18 | 18.9 CH3 | 21.5 CH3 | 19.2 CH3 | 20.0 CH3 | 18.9 CH3 |
| 19 | 29.8 CH2 | 30.2 CH2 | 18.4 CH3 | 29.8 CH2 | 29.8 CH2 |
| 20 | 26.5 CH | 78.6 C | 78.4 C | 31.5 CH | 26.3 CH |
| 21 | 17.7 CH3 | 27.1 CH3 | 27.6 CH3 | 18.5 CH3 | 17.7 CH3 |
| 22 | 26.4 CH2 | 27.2 CH2 | 27.1 CH2 | 33.8 CH2 | 26.4 CH2 |
| 23 | 31.4 CH2 | 22.5 CH2 | 22.5 CH2 | 28.6 CH2 | 31.1 CH2 |
| 24 | 73.8 CH | 69.7 CH | 69.6 CH | 80.3 CH | 75.2 CH |
| 25 | 77.2 C | 76.0 C | 76.0 C | 73.2 C | 73.0 C |
| 26 | 25.6 CH3 | 27.4 CH3 | 27.4 CH3 | 23.1 CH3 | 22.8 CH3 |
| 27 | 25.9 CH3 | 28.1 CH3 | 28.1 CH3 | 26.6 CH3 | 26.8 CH3 |
| 28 | 20.8 CH3 | 20.8 CH3 | 26.1 CH3 | 20.8 CH3 | 20.7 CH3 |
| 20 | 22.2 CH3 | 22.1 CH3 | 21.3 CH3 | 22.2 CH3 | 22.1 CH3 |
| 30 | 20.0 CH3 | 19.9 CH3 | 24.9 CH3 | 19.0 CH3 | 19.9 CH3 |
| OMe | 57.1 CH3 |