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. Author manuscript; available in PMC: 2023 Sep 2.
Published in final edited form as: ACS Catal. 2022 Aug 15;12(17):10581–10586. doi: 10.1021/acscatal.2c03400

Table 2.

Scope of Ketonesa, b

graphic file with name nihms-1897078-t0003.jpg
a

Conditions: 1 (0.1 mmol, 1.0 equiv), methyl 4-iodobenzoate (2.0 equiv), Pd(OAc)2 (10 mol%), TDG1 (30 mol%), L12 (60 mol%), AgTFA (3.0 equiv) and ClCH2COOH (1.5 equiv) in HFIP (0. 5 mL), 120°C, under air, 48 h.

b

Isolated yields.

c

with ClCH2COOH (0.8 equiv) as additive

d

The reaction condition was modified with TDG1 (35 mol%), L10 (80 mol%) and ClCH2COOH (1.2 equiv) in HFIP (0.45 mL).