Table 3. 1H-Decoupled 31P MAS NMR Spectral Deconvolution of the Dry Pellet Mixture.
| SITES |
||||||
|---|---|---|---|---|---|---|
| 1 | 2 | 3 | 4 | 5 | 6 | |
| δ(iso) (ppm) | 7.06 | 6.54 | 4.95 | 4.44 | 3.84 | 2.41 |
| δ(CSA) (ppm) | 62.33 | 80.54 | 59.06 | 62.28 | 23.65 | 67.84 |
| η(CSA) | 0.121 | 0.122 | 0.086 | 0.109 | 0.1 | 0.136 |
| width (Hz) | 104 | 156 | 114 | 125 | 187 | 1500 |
| integrala | 1.02 × 109 | 1.12 × 109 | 5.36 × 109 | 4.41 × 109 | 6.00 × 109 | 2.72 × 109 |
| fraction | 0.049 | 0.054 | 0.260 | 0.214 | 0.291 | 0.132 |
Best overlap 91.65%.