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. 2023 May 4;14(6):802–809. doi: 10.1021/acsmedchemlett.3c00093

Table 1. Composition and HPLC-Retention Times of the Prepared Peptides.

peptide P1 P2 P3 P4 Mw (g/mol) retention time (min)
1 Ph R Tbta R 788.10 9.23
2 Ph R Ph R 580.74 7.61
3 Ph R S-BrW R 698.67 7.98
4 Ph R R-BrW R 698.67 7.62
5 Ph R diBrOMe R 768.56 8.11
6 Ph R OMeBip R 686.86 8.18
7 Ph R diBrOMeBip R 844.65 8.68
8 diBrOMe R diBrOMe R 956.37 8.56
9 BrOMe R BrOMe R 798.58 8.09
10 diBrOH R diBrOH R 928.32 7.77
11 diBrOMe R W R 807.59 8.18
12 diBrOMe R BrW R 886.49 8.43
13 Br-Ind R diBrOMe R 886.49 8.47
14 Ph R Bip KN(Me)3 671.91 8.19
15 Ph R Bip C5N(Me)3 656.90 8.55
16 Ph KN(Me)3 Bip R 671.91 8.20
17 Ph KN(Me)3 Bip KN(Me)3 686.98 8.15
18 Ph R diBrOMe C5N(Me)3 768.62 8.45
19 diBrOMe K diBrOMe K 900.35 8.47
a

Tri-tert-butyl tryptophan.