Table 1.
The intensity data collection method, experimental parameters, and structure determination's final outcomes were based on crystal data.
| CCDC | 2258214 |
| Chemical formulation | C7H12N2O5 |
| Temperature | 150 K |
| Formula weight (g mol−1) | 204.19 |
| Crystal system | Orthorhombic |
| Space group | Pnma |
| a, b, c (Å) | 11.7185(8), 7.2729(6), 11.0163(8) |
| Z | 4 |
| V(Å3) | 938.89(12) |
| F(000) | 432 |
| Radiation type | Mo Kα |
| μ(mm−1) | 0.123 |
| Crystal size (mm) | 0.32 × 0.20 × 0.14 |
| Index ranges | -15≤ h ≤ 14, -9 ≤ k ≤ 9, -14 ≤ l ≤ 14 |
| Reflections collected | 10163 |
| Independent reflections | 1159 |
| Reflections with I > 2σ(I) | 1113 |
| Rint | 0.0424 |
| Diffractometer | D8 Venture (Bruker-AXS) |
| Absorption correction | Multi-scan |
| Tmin, Tmax | 0.900, 0.983 |
| Refined parameters | 84 |
| R[F2 > 2σ(F2)] | 0.0725 |
| wR(F2) | 0.1762 |
| Goodness of fit | 1.254 |
| Δρmax, Δρmin (eÅ−3) | 0.410, −0.293 |