Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.
1H (600 MHz) and 13C (150 MHz) NMR data of compound 1 (CDCl3, J in Hz)
| Position | δC, type | δH | HMBC |
|---|---|---|---|
| 1 | 149.13 | ||
| 2 | 122.45 | ||
| 3 | 151.44 | ||
| 4 | 144.56 | ||
| 5 | 136.41 | ||
| 6 | 112.07 | 6.78 (s, 1H) | C-2, C-5, C-1″ |
| 1′ | 132.62 | ||
| 2′/6′ 3″/5″ | 130.58, 128.39 | 7.44 (m, 4H) | C-1, C-4′ |
| 3′/5′ | 129.46 | 7.53 (m, 2H) | C-1′ |
| 4′ | 128.50 | 7.44 (m, 1H) | C-2′, C-6′ |
| 1″ | 138.10 | ||
| 2″/6″ | 129.34 | 7.59 (m, 2H) | C-4, C-4″ |
| 4″ | 127.53 | 7.36 (m, 1H) | C-2″, C-6″ |
| 5-OCH3 | 61.17 | 3.68 (s, 3H) | C-5 |
| 6-OCH3 | 61.04 | 3.59 (s, 3H) | C-6 |
