Table 5.
This study investigates the catalytic capacity of numerous catalysts present in the given text toward the synthesis of 4f.
Entry | Catalyst | Conditions | Time/yield (%) | References |
---|---|---|---|---|
1 | Cu/Cu2O@g-C3N4 | White LED, EtOH, rt | 4.5 h/86 | 19 |
2 | Na2 eosin Y | White LED, EtOH, rt | 10 min/94 | 22 |
3 | Bakers, yeast | Room temperature | 1440 min/84 | 24 |
4 | Hydrotalcite | Solvent-free, 80 °C | 35 min/84 | 25 |
5 | [Al(H2O)6](BF4)3 | MeCN, Reflux | 1200 min/81 | 26 |
6 | Cu(BF4)2.xH2O | Room temperature | 30 min/90 | 28 |
7 | [Btto][p-TSA] | Solvent-free, 90 °C | 30 min/96 | 29 |
8 | Triethylammonium acetate | Solvent-free,70 °C | 45 min/90 | 30 |
9 | Saccharin | Solvent-free, 80 °C | 15 min/88 | 31 |
10 | Caffeine | Solvent-free, 80 °C | 25 min/91 | 32 |
11 | 4CzIPN | Blue LED, EtOH, rt | 5 min/96 | 36 |
12 | CsPbBr3 | Blue LED, EtOH, rt | 5 min/93 | This work |
The synthesis employs three distinct constituents namely benzaldehyde, ethyl acetoacetate, and urea.