Table 3.
Cyclization of other adducts 4.
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Entry | R1 | R2 | Yield [%] | Recovery of 4/% | |||
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1 | 8 | 11 | |||||
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1 | Me | OEt | c | 8 | 39 | 0 | 0 |
2 | Et | OMe | d | 12 | 44 | trace | 0 |
3 | iPr | OMe | e | 24 | 36 | 9 | 0 |
4 | Ph | OEt | f | 56 | 9 | 17 | 0 |
5 | Me | Me | b | 0 | 21 | 0 | 17 |
6 | Me | Ph | g | 5 | 30a | 0 | 7 |
aTotal yield of two isomers 8g (14%) and 8g’ (R1 = Ph, R2 = Me, 16%).