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. 2023 May 16;3(6):1539–1553. doi: 10.1021/jacsau.3c00014

Scheme 11. Scalable Synthesis of BCP Sulfones from Sulfonyl Halides (Anderson et al.33).

Scheme 11

BnNMe3ICI2 was used as iodinating agent.

Br2 was used as brominating agent, 10 mol % Et3B was also added, and the reaction with 6 was performed over 2 h.