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. 2023 May 31;11(6):498. doi: 10.3390/toxics11060498
No. Compound MU 0.3 ng/mL 1.25 ng/mL 5 ng/mL 20 ng/mL 40 ng/mL
Precision (RSD %) Precision (RSD %) Precision (RSD %) Precision (RSD %) Precision (RSD %)
Rec. (%) Intraday Interday Rec. (%) Intraday Interday Rec. (%) Intraday Interday Rec. (%) Intraday Interday Rec. (%) Intraday Interday
1 2-Phenylphenol 22.71 111.20 11.92 11.29 93.26 17.78 20.06 100.24 17.65 18.54 98.44 7.68 8.21
2 4,4′-Dichlorobenzophenone (metabolite of dicofol) 24.86 93.72 17.18 19.30 113.48 15.09 14.00 89.56 13.23 15.55 99.40 14.69 15.56 103.47 8.37 8.51
3 Abamectine 31.79 97.94 13.71 14.74 98.51 11.04 11.80 101.43 10.98 11.40
4 Acenaphthene 25.01 94.41 15.26 17.02 97.82 4.08 4.40 94.69 11.06 12.29 96.61 18.23 19.86 101.84 8.60 8.89
5 Acenaphtylene 33.02 114.97 21.82 19.98 100.11 14.39 15.13 98.15 18.65 20.01 98.35 11.22 12.00
6 Acephate 16.55 97.41 9.85 10.65 98.76 3.85 4.10 101.74 5.62 5.82
7 Acetaminophen (Paracetemol) 16.63 118.40 15.13 13.45 87.58 11.04 13.27 99.23 7.33 7.77 102.05 5.61 5.78
8 Acetamiprid 7.32 107.58 10.19 9.97 98.11 2.90 3.11 94.21 6.35 7.09 102.36 4.51 4.64 99.41 2.48 2.63
9 Acrinathrin 25.44 87.18 12.90 15.57 96.81 13.01 14.15 100.45 8.45 8.86 98.88 8.67 9.23
10 Albendazole 10.42 93.43 7.73 8.70 104.12 3.76 3.81 102.98 4.43 4.52 103.28 5.39 5.50 96.07 2.30 2.52
11 Aldicarb 9.06 99.93 8.50 8.95 98.97 1.74 1.85 98.05 6.31 6.77 102.21 4.94 5.09 98.22 2.84 3.05
12 Aldicarb-sulfone 8.85 105.03 3.63 3.64 90.04 3.36 3.92 98.99 6.72 7.14 102.24 2.66 2.74
13 Aldicarb-sulfoxide 6.33 116.10 6.35 5.75 90.44 5.73 6.66 99.84 3.55 3.75 101.22 2.02 2.10
14 Aldrin 31.42 106.18 18.16 18.01 106.69 16.86 16.64 88.98 15.53 18.37 95.66 8.75 9.63 102.90 10.79 11.04
15 Anthracene 18.57 100.98 10.68 11.14 96.33 11.81 12.91 92.18 9.84 11.24 103.89 5.92 6.00
16 Atrazine 10.31 96.11 3.58 3.92 105.40 2.88 2.88 101.07 6.81 7.10 102.47 4.20 4.32 97.19 2.93 3.17
17 Azinphos-methyl 8.39 101.15 8.53 8.88 103.85 6.77 6.86 99.07 10.10 10.73 102.81 4.28 4.38 97.24 2.15 2.32
18 Azoxystrobin 10.50 98.04 6.27 6.73 104.37 2.98 3.01 97.56 6.32 6.82 99.06 5.25 5.58 100.42 3.61 3.79
19 BDE-28 36.70 104.31 14.98 15.12 101.58 7.56 7.83 90.05 16.18 18.91 93.67 13.52 15.19 105.17 12.45 12.46
20 BDE-47 32.46 99.47 11.23 11.88 111.52 2.64 2.49 96.16 15.98 17.49 97.65 14.95 16.12 100.18 11.19 11.75
21 BDE-85 58.35 94.45 19.12 21.30 104.21 17.67 17.85 92.60 10.45 11.88 94.08 10.62 11.89 100.70 20.16 21.08
22 BDE-99 42.81 104.66 20.57 20.68 103.83 13.88 14.08 90.67 12.91 14.99 90.83 10.23 11.86 105.41 14.66 14.63
23 BDE-100 52.30 96.85 12.38 13.46 107.88 19.14 18.67 96.30 17.82 19.48 97.14 10.98 11.90 99.85 18.00 18.97
24 BDE-153 36.24 102.12 18.29 18.85 104.09 16.37 16.56 95.49 18.09 19.94 99.65 14.59 15.41 101.80 12.53 12.96
25 BDE-154 43.70 97.71 13.27 14.29 105.03 20.19 20.24 93.86 10.08 11.31 95.11 9.40 10.41 101.40 15.13 15.70
26 BDE-183 59.57 108.60 11.54 11.18 101.10 23.51 24.48 89.53 4.87 5.73 100.61 15.10 15.80 101.56 20.65 21.40
27 Benalaxyl 11.73 101.52 14.48 15.01 101.59 4.49 4.65 95.51 4.74 5.22 100.23 4.63 4.86 99.99 4.04 4.25
28 Bendiocarb 8.45 105.79 7.77 7.73 95.96 4.86 5.33 97.21 5.10 5.52 102.51 5.03 5.16 98.61 2.73 2.91
29 Bendiocarb metabolite (2, 2-dimethylbenzo-1, 3-dioxol-4-ol) 54.51 96.61 12.05 13.13 92.35 5.16 5.89 102.37 18.93 19.47
30 Benfuracarb 52.63 97.77 12.48 13.43 112.31 14.78 13.85 105.31 20.90 20.89 95.61 17.44 19.20
31 Benzo[a]anthracene 23.00 100.95 13.34 13.91 104.58 7.80 7.85 86.86 12.31 14.92 104.46 13.94 14.04 97.66 7.66 8.26
32 Benzo[a]pyrene 18.97 97.86 14.37 15.46 105.41 9.73 9.71 90.28 17.88 20.85 96.05 8.26 9.06 101.85 6.47 6.68
33 Benzo[b]fluoranthene 37.06 107.89 12.46 12.16 100.81 14.27 14.90 91.94 9.57 10.95 91.76 11.46 13.15 105.88 12.46 12.39
34 Benzo[ghi]perylene 39.89 96.46 10.58 11.55 103.87 8.89 9.01 98.58 13.31 14.21 97.68 10.19 10.98 100.50 13.77 14.42
35 Benzo[k]fluoranthene 31.40 99.90 21.36 22.51 107.59 7.48 7.32 85.41 21.81 23.88 93.19 8.18 9.24 104.38 10.62 10.71
36 Bifenthrin 25.99 107.06 8.54 8.40 109.66 6.37 6.11 90.40 11.88 13.84 103.20 9.74 9.94 98.16 8.77 9.41
37 Bitertanol 8.81 101.72 22.45 23.23 106.23 12.39 12.28 90.03 3.62 4.23 99.49 5.66 5.99 101.65 2.84 2.94
38 Boscalid (formerly nicobifen) 47.03 100.63 19.36 20.25 104.11 8.22 8.31 89.07 12.48 14.74 95.12 16.20 17.93 103.61 16.30 16.56
39 Brodifacoum 28.30 84.19 11.76 14.71 103.80 13.59 13.78 94.44 11.45 12.76 103.36 10.95 11.15 98.97 9.67 10.28
40 Bromadiolone 25.02 90.11 18.91 22.09 95.42 11.38 12.56 94.54 4.72 5.25 102.52 12.54 12.87 99.43 8.58 9.09
41 Bromopropylate 39.80 103.98 10.96 11.09 110.51 9.16 8.73 86.70 15.43 18.73 104.76 15.06 15.13 99.66 13.68 14.45
42 Bromuconazole (two isomers) 30.91 106.55 15.23 15.17 108.81 10.70 10.20 87.97 14.45 17.32 96.38 14.51 15.79 103.14 10.58 10.82
43 Bupirimate 10.85 85.46 18.36 22.62 104.46 4.39 4.42 105.85 10.88 10.82 102.49 6.13 6.30 96.40 2.74 2.99
44 Buprofezin 18.10 95.66 3.40 3.74 107.59 7.25 7.10 96.26 5.46 5.97 99.52 5.86 6.20 100.45 6.24 6.54
45 Cadusafos (ebufos) 20.57 87.81 8.36 10.02 117.52 6.95 6.23 108.46 4.48 4.35 104.39 6.46 6.51 93.16 5.09 5.75
46 Carbaryl 11.55 97.61 7.53 8.12 97.44 2.60 2.81 99.40 7.22 7.65 101.88 5.76 5.95 97.76 3.62 3.90
47 Carbendazim (azole) 10.14 101.48 21.84 22.65 102.71 2.20 2.26 97.10 5.65 6.12 103.15 2.87 2.93 97.85 3.13 3.37
48 Carbofuran 9.94 93.67 4.44 4.98 102.64 3.52 3.61 100.79 5.85 6.11 102.98 3.43 3.51 96.87 2.61 2.84
49 Carbofuran-3-hydroxy 10.85 104.10 6.64 6.72 90.76 7.16 8.31 100.99 1.16 1.21 100.99 3.69 3.85
50 Cefuroxima axetil (two isomers) 10.45 107.63 10.02 9.80 97.71 3.85 4.14 92.71 5.91 6.71 102.92 5.68 5.81 99.41 3.57 3.78
51 Chloramphenicol 15.42 88.16 14.23 16.99 98.52 14.68 15.68 101.47 5.25 5.45
52 Chlorantraniliprole 9.55 108.96 15.78 15.25 99.65 6.49 6.86 95.00 6.38 7.06 101.51 3.72 3.85 99.52 3.26 3.45
53 Chlorfenapyr 11.15 96.05 11.01 12.06 104.19 12.01 12.14 95.66 14.47 15.92 101.29 3.76 3.91
54 Chlorfenvinphos 15.13 93.08 16.18 18.30 107.34 2.55 2.50 103.43 4.19 4.26 103.44 6.18 6.29 95.44 4.05 4.47
55 Chlorobenzilate 21.05 97.87 14.12 15.19 108.68 7.88 7.63 98.29 16.88 18.07 95.40 12.29 13.56 101.32 7.24 7.52
56 Chlorophacinone 55.65 94.25 20.33 24.10 105.39 13.83 13.81 100.36 19.20 20.14
57 Chlorpropham 39.94 92.73 11.96 13.57 110.61 9.51 9.05 96.09 13.80 15.12 98.45 14.97 16.00 100.46 13.78 14.44
58 Chlorpyrifos 39.83 92.57 15.38 17.49 105.52 8.87 8.85 92.26 16.56 18.89 96.32 10.16 11.10 103.09 13.77 14.06
59 Chlorpyrifos methyl 9.93 92.64 15.61 17.73 107.15 8.33 8.18 94.06 15.62 17.48 96.37 16.97 18.54 103.83 2.22 2.25
60 Chlorthal dimethyl 41.20 88.50 10.56 12.56 106.05 10.65 10.58 93.19 12.01 13.57 103.42 12.83 13.06 97.54 13.90 15.00
61 Chrysene 12.16 108.26 2.41 2.34 94.17 4.88 5.46 99.74 5.92 6.25 100.65 4.18 4.37
62 Clindamycin 12.54 72.04 14.13 20.64 112.63 14.50 13.56 108.56 7.37 7.14 102.46 5.05 5.19 95.27 2.77 3.06
63 Clofentezine 7.68 99.14 24.98 24.52 94.91 9.26 10.27 101.49 5.13 5.32 99.88 2.64 2.78
64 Clothianidin 10.99 98.28 11.10 11.89 97.34 9.80 10.60 100.77 5.37 5.61 99.70 3.77 3.98
65 Cortiscosterone 21 acetate 22.42 94.83 18.73 20.79 105.17 22.77 22.79 109.51 13.73 13.20 95.93 7.04 7.72
66 Coumachlor 21.24 107.31 11.49 11.27 107.08 7.04 6.92 103.11 6.14 6.27 95.47 6.46 7.12
67 Coumaphos 12.93 95.94 19.86 21.79 93.39 15.06 16.97 101.10 6.93 7.21 99.47 4.42 4.68
68 Coumatetralyl 10.65 100.62 2.32 2.43 102.04 11.53 11.89 102.08 6.66 6.87 97.23 3.08 3.34
69 Cyazofamid 13.81 93.47 12.35 13.91 99.45 5.13 5.43 103.02 6.37 6.51 101.38 5.49 5.70 97.05 4.23 4.59
70 Cyflufenamid 37.37 96.60 10.58 11.53 92.95 11.22 12.71 103.79 12.85 13.03
71 Cyfluthrin (sum of four isomers) 24.66 98.74 12.55 13.37 101.21 6.88 7.16 100.31 8.50 8.92
72 Cyhalothrin (lambda isomer) 10.29 107.25 5.73 5.62 95.42 6.79 7.49 101.83 4.31 4.46 99.67 3.53 3.73
73 Cymoxanil 36.58 105.21 4.95 4.95 94.59 8.18 9.11 98.88 16.00 17.03 101.34 12.65 13.14
74 Cypermethrin (sum of four isomers) 10.29 105.20 7.63 7.64 96.50 5.24 5.71 95.78 8.25 9.07 100.63 6.82 7.13 99.76 3.54 3.73
75 Cyproconazole (two isomers) 15.50 104.49 8.19 8.25 99.15 9.59 10.18 104.91 11.76 11.80 97.82 5.06 5.45
76 Cyprodinil 7.00 92.46 12.18 13.86 100.99 7.51 7.83 99.58 2.39 2.53
77 Cyromazine 42.82 103.52 9.90 10.06 97.41 24.47 24.44 116.05 20.00 18.14
78 Danofloxacin 23.86 75.98 14.99 20.77 117.29 12.71 11.40 93.72 15.08 16.94 105.40 16.03 16.01 97.73 7.97 8.58
79 Dazomet 13.54 95.56 19.38 21.35 103.50 6.07 6.17 95.26 12.19 13.47 99.29 13.17 13.96 100.39 4.66 4.89
80 Deltamethrin 33.46 93.86 20.04 22.47 105.04 15.85 15.88 92.37 16.09 18.34 92.78 13.85 15.71 109.54 9.91 9.52
81 Demeton-S-methyl 47.32 116.16 12.82 11.62 89.95 16.43 19.23 98.03 24.66 24.48 93.53 22.92 23.79
82 Demeton-S-methyl-sulfone (Dioxydemeton) 39.00 111.73 11.57 10.90 90.66 10.87 12.62 100.51 13.73 14.38 100.55 13.46 14.09
83 Dexamethasone 11.06 92.13 8.53 9.75 105.54 7.70 7.68 101.60 6.30 6.53 101.94 5.30 5.47 97.20 3.23 3.50
84 Diazinon 3.06 92.46 6.30 7.18 93.38 3.99 4.50 101.49 5.21 5.41 100.06 1.05 1.11
85 Dibenzo[a,h]anthracene 16.68 112.64 14.38 13.43 90.03 10.00 11.69 97.97 7.56 8.12 101.52 5.69 5.90
86 Dichlorodiphenyldichloroethane (p,p′ DDD) 37.62 95.53 16.47 18.15 107.32 7.25 7.11 89.48 15.34 18.05 90.24 18.81 21.94 106.76 12.50 12.32
87 Dichlorodiphenyldichloroethylene (p,p′ DDE) 34.11 106.07 13.76 13.66 99.57 8.40 8.88 94.20 14.12 15.78 98.30 8.73 9.35 101.23 11.79 12.26
88 Dichlorodiphenyltrichloroethane (p,p′ DDT) 14.94 108.60 4.09 3.97 90.66 14.41 16.73 103.97 14.16 14.34 99.70 5.13 5.42
89 Diclofenac 11.14 105.64 4.06 4.05 93.24 5.48 6.18 99.12 4.97 5.28 101.60 3.70 3.84
90 Dicloran 10.23 100.39 22.88 23.99 105.92 7.34 7.29 98.48 3.34 3.57
91 Diclorvos 38.24 111.23 23.60 22.33 93.47 17.10 19.26 94.62 11.43 12.72 102.13 13.23 13.64
92 Dieldrin 11.43 98.64 14.64 15.62 102.41 3.65 3.75 96.37 6.18 6.75 100.66 6.97 7.29 99.81 3.93 4.14
93 Diethathyl ethyl 14.86 88.24 7.95 9.48 108.70 2.58 2.50 105.93 3.97 3.95 102.90 4.63 4.73 95.31 3.87 4.27
94 Diethofencarb 20.11 102.72 17.08 17.51 101.57 3.86 4.00 99.43 8.58 9.09 102.32 9.12 9.38 97.62 6.64 7.16
95 Difenacoum 12.25 80.96 11.55 15.01 102.72 5.45 5.59 100.39 8.05 8.44 102.92 4.94 5.05 97.20 3.69 4.00
96 Difenoconazole 19.48 102.74 14.93 15.30 101.47 14.00 14.52 103.11 9.15 9.34 96.67 6.19 6.74
97 Difethialone 45.00 101.59 7.31 7.58 94.70 14.77 16.42 103.05 15.60 15.93
98 Difloxacin 19.08 90.37 18.36 21.39 102.44 15.11 23.80 105.09 11.28 11.30 96.33 5.94 6.49
99 Diflubenzuron 25.99 96.88 18.65 20.26 107.54 14.71 14.39 97.24 17.62 22.90 96.41 10.42 11.37 103.53 8.77 8.92
100 Diflufenican 10.75 96.03 3.56 3.91 104.44 1.69 1.70 97.50 5.98 6.45 99.88 5.87 6.18 100.00 3.70 3.90
101 Dimethenamid-P (and its R-isomer) 9.82 102.25 5.36 5.51 95.04 6.05 6.70 101.97 4.95 5.11 99.49 3.36 3.55
102 Dimethoate 12.67 94.43 16.66 18.57 100.31 6.33 6.64 101.63 9.07 9.40 101.57 7.88 8.16 97.78 4.04 4.35
103 Dimethomorph (two isomers) 37.37 89.48 12.23 14.39 111.11 7.12 6.74 93.84 17.37 19.49 95.28 10.47 11.57 103.95 12.83 12.99
104 Dimethylphenylsulfamide (DMSA, metabolite of dichlofluanid) 24.15 111.52 19.40 18.31 99.56 6.10 6.45 89.53 13.95 16.40 94.14 12.44 13.91 104.15 7.98 8.06
105 Diniconazole-M 25.63 98.33 21.68 23.21 105.75 11.68 11.62 102.36 11.88 12.21 96.91 8.42 9.15
106 Dinocap 54.01 106.98 18.75 18.45 90.90 9.62 11.14 104.03 18.77 18.99
107 Diphacinone 30.26 70.85 17.52 19.03 105.76 17.44 17.36 95.74 15.70 17.26 97.12 16.78 18.18 101.09 10.45 10.88
108 Diphenylamine 30.91 101.83 7.15 7.39 96.13 10.34 11.32 101.68 9.00 9.32 99.37 10.60 11.23
109 N,N-dimethylformamidine (DMF, metabolite of amitraz) 26.22 94.68 6.70 7.45 103.33 11.73 11.94 97.94 8.82 9.48
110 Dodine 11.59 110.75 4.01 3.81 93.52 7.93 8.93 100.22 6.75 7.09 100.39 3.99 4.18
111 Endosulfan alfa 17.85 98.84 3.86 4.11 100.61 4.54 4.75 101.95 7.04 7.27 97.48 5.82 6.28
112 Endosulfan beta 8.72 91.54 6.43 7.39 100.39 5.32 5.57 103.11 6.74 6.88 97.25 2.30 2.49
113 Endosulfan sulfate 44.34 102.03 12.59 12.99 106.47 16.24 16.06 91.46 14.51 16.70 98.19 11.21 12.02 102.13 15.37 15.84
114 Endrin 28.51 105.62 11.47 11.43 104.87 14.89 14.94 90.35 12.35 14.39 97.33 10.72 11.59 103.11 9.73 9.94
115 Enrofloxacin 49.49 115.11 10.88 9.95 92.23 10.15 11.58 90.60 16.66 19.36 101.21 23.80 24.76 103.66 24.24 24.62
116 EPN 30.69 118.43 4.97 4.42 93.36 21.86 24.65 96.81 15.31 16.65 106.31 9.94 9.84
117 Epoxiconazole 44.58 98.81 18.22 19.41 96.32 24.41 24.67 103.51 22.51 22.89
118 Eprinomectin 47.23 109.58 10.88 10.45 99.07 6.16 6.54 86.37 12.62 15.38 103.27 17.33 17.67 98.92 16.16 17.19
119 Eritromicin 10.61 112.06 10.02 9.42 95.45 5.64 6.23 92.98 7.30 8.26 101.46 5.40 5.60 99.72 3.64 3.85
120 Esfenvalerate 47.92 99.09 14.55 15.45 94.54 8.79 9.78 91.95 14.85 17.00
121 Ethion (diethion) 17.38 107.84 6.55 6.40 100.92 3.32 3.47 94.93 4.63 5.13 102.77 6.04 6.19 98.59 5.86 6.26
122 Ethirimol 28.11 97.99 14.21 15.26 94.70 16.88 18.77 98.41 12.08 12.92 101.62 9.70 10.05
123 Ethofumesate 16.21 91.25 11.64 13.43 110.47 4.31 4.11 106.91 6.92 6.81 102.24 5.81 5.98 95.56 4.56 5.02
124 Ethoprophos 10.21 101.69 2.29 2.37 92.72 7.46 8.47 102.49 4.21 4.32 99.82 3.51 3.70
125 Etofenprox 53.62 100.20 15.93 16.73 109.55 5.22 5.02 92.07 14.26 16.30 98.97 18.40 19.57 109.18 18.13 17.48
126 Etoxazole 12.52 82.17 11.50 14.74 106.77 4.94 4.87 103.52 6.52 6.63 102.93 5.05 5.17 95.93 3.20 3.52
127 Famoxadone 29.18 85.42 14.45 17.81 115.74 6.23 5.67 94.81 12.30 13.65 98.59 14.01 14.96 100.27 10.06 10.56
128 Fenamidone 34.54 96.20 9.43 10.31 106.75 3.34 3.29 97.38 5.53 5.98 97.70 6.43 6.93 104.34 11.77 11.87
129 Fenamiphos 16.04 103.97 16.68 16.89 98.60 13.26 14.16 103.76 6.17 6.26 96.77 4.97 5.40
130 Fenamiphos sulfone 21.54 79.80 11.11 14.66 104.85 11.91 11.95 104.61 13.51 13.59 102.75 7.74 7.93 95.11 6.43 7.12
131 Fenamiphos sulfoxide 13.37 103.04 14.97 15.29 97.12 7.01 7.60 98.03 12.13 13.02 100.27 6.16 6.46 99.91 4.60 4.85
132 Fenarimol 15.17 107.00 8.52 8.38 102.18 3.35 3.45 93.40 6.06 6.83 100.78 6.32 6.60 100.05 5.23 5.50
133 Fenazaquin 13.05 105.73 16.63 16.56 96.32 6.58 7.19 99.41 5.94 6.29 99.69 4.48 4.73
134 Fenbendazole 42.78 96.23 19.95 21.82 109.39 5.34 5.14 89.90 10.82 12.66 95.35 17.12 18.90 93.89 13.64 15.30
135 Fenbuconazole 19.60 98.06 10.35 11.12 102.23 3.41 3.51 96.79 6.16 6.70 98.96 6.15 6.54 100.65 6.76 7.07
136 Fenbutatin oxide 10.78 97.94 8.11 8.72 99.88 1.64 1.73 103.72 7.34 7.44 103.52 7.08 7.20 95.97 2.41 2.64
137 Fenhexamid 40.07 90.08 8.82 10.30 114.44 14.05 12.92 94.27 11.50 12.84 93.50 13.12 14.77 103.85 13.81 14.00
138 Fenitrothion 40.91 95.76 12.40 13.64 95.28 7.34 8.11 91.70 5.97 6.85 99.29 10.07 10.68 101.66 14.16 14.66
139 Fenoxycarb 12.29 86.84 13.72 16.63 91.58 17.17 19.73 100.48 9.06 9.49 99.83 4.23 4.46
140 Fenpropathrin 35.65 86.56 20.78 24.27 81.25 14.38 18.63 98.13 18.26 19.58 103.85 12.22 12.39
141 Fenpropidin 12.15 95.06 6.49 7.19 106.46 8.00 7.91 105.99 8.98 8.92 102.43 7.54 7.75 95.33 2.61 2.88
142 Fenpropimorph 35.90 103.28 13.33 13.58 90.34 13.75 16.02 103.55 6.98 7.09 97.50 12.08 13.04
143 Fenpyroximate 12.14 95.44 5.24 5.78 101.85 2.69 2.78 102.16 7.02 7.24 101.62 6.06 6.28 97.48 3.75 4.05
144 Fenthion 9.38 90.36 7.35 8.56 98.88 2.96 3.15 97.47 6.22 6.72 102.02 6.88 7.10 97.91 2.86 3.08
145 Fenthion oxon 10.55 84.90 13.69 16.97 103.86 2.51 2.55 104.88 6.93 6.95 103.80 6.09 6.18 95.42 1.75 1.93
146 Fenthion oxon sulfone 20.43 96.71 11.10 12.08 102.96 5.14 5.25 88.90 15.24 18.05 99.53 6.94 7.34 101.39 7.02 7.29
147 Fenthion oxon sulfoxide 9.90 85.66 11.30 13.88 105.85 4.41 4.39 101.77 5.58 5.78 102.66 5.41 5.54 96.46 2.33 2.55
148 Fenthion sulfone 10.05 107.97 6.70 6.53 92.79 4.16 4.71 100.24 5.77 6.06 100.92 3.42 3.57
149 Fenthion sulfoxide 7.50 99.96 4.85 5.10 92.76 6.52 7.39 101.15 5.18 5.39 99.99 2.58 2.72
150 Fenvalerate 18.02 106.51 10.34 10.22 94.20 4.12 4.60 100.52 7.73 8.10 100.12 6.21 6.53
151 Fipronil 10.85 102.94 2.32 2.37 96.57 4.16 4.54 101.76 6.99 7.23 98.21 3.49 3.74
152 Fipronil sulfide 27.97 100.06 11.14 11.72 96.61 12.67 13.81 98.42 12.29 13.14 100.61 9.65 10.10
153 Flocoumafen 32.20 103.31 18.68 19.03 106.30 11.28 11.17 84.22 19.69 24.61 92.29 17.76 20.25 106.01 10.60 10.52
154 Fluazinam 46.45 114.73 14.06 12.90 95.47 20.10 22.16 92.11 16.31 18.64 103.77 16.09 16.32
155 Flubendiamide 24.22 86.88 15.73 19.06 102.45 7.19 7.38 105.55 9.72 9.70 103.52 13.19 13.41 94.98 7.38 8.18
156 Flucythrinate (two isomers) 10.65 100.27 9.51 9.98 96.64 4.82 5.25 100.57 5.45 5.70 100.22 3.67 3.85
157 Fludioxonil 8.71 104.15 20.63 20.85 95.66 13.35 14.69 103.64 8.36 8.49 97.76 2.54 2.74
158 Flufenoxuron 33.79 98.86 17.23 18.38 109.09 6.89 6.63 88.18 11.93 14.25 96.14 14.12 15.49 100.17 11.63 12.25
159 Flumequine 38.28 91.35 16.93 19.51 109.03 17.09 16.50 95.00 11.81 13.08 96.70 9.83 10.70 107.39 12.61 12.36
160 Flunixin 27.62 97.46 6.48 7.00 107.67 9.38 9.17 103.82 9.75 9.89 95.15 8.67 9.59
161 Fluopyram 21.85 105.27 4.00 4.00 96.44 4.45 4.86 102.22 5.46 5.63 103.09 6.89 7.04 97.63 7.25 7.82
162 Fluoranthene 13.72 104.43 8.69 8.76 100.36 3.65 3.83 104.45 4.68 4.72 96.53 4.00 4.36
163 Fluorene 20.70 101.43 23.18 24.05 113.31 18.05 16.77 89.67 14.11 16.57 98.30 14.65 15.69 101.25 7.12 7.41
164 Fluquinconazole 29.95 95.42 20.55 22.67 100.08 8.51 8.95 90.35 13.57 15.81 98.39 14.17 15.16 101.82 10.33 10.68
165 Flusilazole 32.98 126.43 13.07 10.88 97.89 10.72 11.52 97.24 23.61 24.55 100.38 11.38 11.93
166 Flutolanil 60.00 92.66 12.40 14.08 101.18 14.94 15.54 95.13 19.18 21.22 93.62 15.30 17.20 101.91 20.93 21.62
167 Flutriafol 16.79 86.68 17.60 21.37 96.15 16.21 17.75 106.59 16.32 16.11 103.95 5.99 6.07 95.04 4.54 5.03
168 Fluvalinate tau 11.32 92.52 12.02 13.68 106.67 5.42 5.35 96.33 5.22 5.70 100.64 5.53 5.78 99.84 3.89 4.11
169 Fonofos 24.20 90.07 8.01 9.36 108.25 4.63 4.50 94.23 12.72 14.21 98.24 7.48 8.01 101.48 8.34 8.65
170 Formetanate 41.20 99.70 3.01 3.18 93.95 8.37 9.38 96.01 13.07 14.33 101.90 14.27 14.74
171 Fosthiazate 28.65 89.32 16.62 19.59 101.72 6.97 7.22 90.25 10.09 11.77 93.78 16.03 17.99 106.61 9.04 8.93
172 Heptachlor 56.79 98.56 14.43 15.41 104.04 21.87 22.13 99.77 19.53 20.61
173 Hexachlorobencene 10.35 95.58 6.30 6.94 101.59 1.16 1.20 99.57 6.00 6.34 102.20 5.31 5.47 97.65 3.14 3.38
174 Hexachlorocyclohexane (alpha) 29.68 100.23 18.01 18.91 101.88 7.48 7.73 86.97 13.33 16.13 97.06 15.73 17.06 104.25 10.01 10.10
175 Hexachlorocyclohexane (beta) 37.80 87.87 7.48 8.96 105.32 11.04 11.03 96.62 14.46 15.76 103.13 20.13 20.55 108.95 11.97 11.57
176 Hexachlorocyclohexane (delta) 8.40 92.16 12.43 14.19 101.83 9.13 9.44 89.92 14.21 16.64 102.61 14.75 15.13 100.23 2.89 3.04
177 Hexaclorocyclohexane (gamma, lindane) 29.92 100.36 8.08 8.47 103.61 10.52 10.69 96.46 21.78 23.76 99.08 20.02 21.28 102.03 10.31 10.64
178 Hexaconazole (two isomers) 31.46 100.10 10.03 10.55 88.50 11.45 13.62 97.93 18.94 20.36 103.54 10.75 10.93
179 Hexaflumuron 35.88 97.06 9.57 10.38 113.20 23.40 21.76 92.15 10.14 11.58 96.83 10.30 11.20 103.17 12.36 12.61
180 Hexythiazox 15.43 97.80 10.18 10.95 105.35 8.07 8.06 104.96 5.88 5.89 94.59 3.67 4.09
181 Imazalil (enilconazole) 18.45 97.75 14.01 15.09 101.04 5.97 6.22 100.01 7.81 8.22 101.55 6.69 6.94 97.44 6.02 6.50
182 Imidacloprid 7.84 101.35 22.14 22.99 98.35 3.04 3.25 92.25 5.84 6.66 101.60 6.37 6.60 100.02 2.70 2.84
183 Indeno [1,2,3-cd] pyrene 12.29 97.23 11.55 12.50 92.72 10.42 11.83 98.82 4.88 5.20 101.76 4.09 4.24
184 Indoxacarb 32.38 99.75 15.92 16.80 106.45 6.90 6.82 95.30 14.81 16.36 102.04 15.42 15.91 99.49 11.11 11.76
185 Iprodione 26.46 97.52 2.64 2.85 95.46 9.30 10.25 103.31 11.12 11.33 98.00 8.91 9.57
186 Iprovalicarb 48.25 103.44 9.99 10.17 86.34 15.08 18.38 101.33 23.37 24.28 97.77 16.35 17.60
187 Isocarbophos 16.58 81.00 9.98 12.97 111.09 0.64 0.61 107.48 7.55 7.39 104.41 5.94 5.98 93.67 3.56 4.00
188 Isofenphos methyl 26.73 90.40 17.60 20.50 113.42 13.97 12.96 92.51 16.14 18.37 95.85 11.95 13.12 102.59 9.15 9.39
189 Isoprothiolane 10.92 102.55 14.09 14.46 100.61 2.07 2.17 99.19 7.14 7.58 100.34 5.36 5.63 99.87 3.76 3.96
190 Ivermectin B1a 16.57 89.05 14.13 16.70 112.83 15.13 14.12 94.12 10.84 12.12 96.43 7.65 8.35 102.21 5.56 5.73
191 Josamycin 43.99 101.89 20.70 21.39 99.76 11.29 11.91 101.30 11.89 12.35 99.69 15.12 15.97
192 Ketoprofen 15.53 114.79 8.64 7.93 97.82 4.08 4.39 94.19 4.56 5.10 101.27 6.16 6.40 100.54 5.35 5.60
193 Kresoxim methyl 9.41 102.73 18.09 18.53 97.66 8.80 9.49 97.14 6.24 6.76 101.48 3.10 3.21
194 Leptophos 18.10 99.43 13.59 14.39 101.04 16.02 16.69 104.54 5.93 5.97 96.08 5.50 6.03
195 Levamisole 56.89 105.30 19.15 19.14 93.77 8.40 9.43 85.56 10.53 12.95 95.50 15.78 17.39 104.79 19.78 19.87
196 Lincomycin 12.57 93.07 12.69 14.36 99.86 11.37 11.98 98.92 2.42 2.58 100.26 4.33 4.55
197 Linuron 23.14 106.60 13.65 13.48 99.47 6.16 6.52 97.09 13.74 14.90 101.71 7.95 8.23
198 Lufenuron 38.43 96.22 15.91 17.40 94.36 21.11 23.55 93.60 21.32 23.11 105.14 13.09 13.10
199 Malaoxon 9.79 101.17 7.70 8.01 97.98 9.53 10.24 103.11 4.58 4.68 97.64 2.92 3.14
200 Malathion 11.22 82.62 13.11 16.71 100.25 6.92 7.26 105.86 13.54 13.47 102.32 7.46 7.68 95.75 2.46 2.71
201 Mandipropamid 12.89 93.28 5.57 6.29 105.42 0.28 0.28 103.46 5.54 5.63 102.64 4.44 4.55 96.42 3.62 3.95
202 Mebendazole 14.17 101.04 17.64 18.38 103.15 3.49 3.56 96.36 6.42 7.01 100.18 4.99 5.25 99.95 4.88 5.14
203 Mefenamic acid 13.26 90.24 9.15 10.67 108.42 3.34 3.24 101.01 6.31 6.57 103.48 6.31 6.42 95.81 3.46 3.80
204 Mefenoxam (metalaxyl-M) 10.25 103.36 12.88 13.12 102.13 3.34 3.44 96.29 5.54 6.06 101.36 5.62 5.83 99.72 3.52 3.72
205 Meloxicam 27.03 111.41 23.58 22.28 87.66 7.84 9.41 101.76 10.58 10.95 99.94 9.31 9.80
206 Mepanipyrim 13.48 97.45 11.59 12.52 104.03 4.06 4.10 96.00 5.27 5.78 100.55 4.75 4.97 99.83 4.64 4.89
207 Mepiquat 20.05 104.81 8.31 8.34 91.46 8.61 9.90 98.44 4.48 4.79 100.48 6.91 7.24
208 Metaflumizone 34.41 116.29 9.64 8.72 88.22 13.33 15.90 95.73 10.36 11.39 103.80 11.78 11.95
209 Metalaxyl 9.37 102.27 7.69 7.92 92.08 6.45 7.37 100.44 7.75 8.12 100.70 3.20 3.35
210 Metaldehyde 24.07 105.40 9.77 9.76 102.17 7.06 7.27 97.79 4.17 4.49 99.76 4.73 4.99 100.25 8.30 8.71
211 Metconazole 20.49 104.02 15.43 15.62 108.15 9.70 9.44 91.84 10.50 12.03 98.19 11.35 12.16 101.68 7.02 7.27
212 Methamidophos (two isomers) 2.94 110.87 18.67 17.72 90.48 6.12 7.12 100.47 2.55 2.68 100.92 0.80 0.83
213 Methidathion 11.98 97.05 8.53 9.25 103.75 4.62 4.69 99.93 6.66 7.01 98.82 4.46 4.75 100.30 4.13 4.33
214 Methiocarb 15.30 93.85 7.21 8.09 98.11 7.61 8.16 101.60 5.20 5.38
215 Methiocarb-sufone 8.59 95.91 4.45 4.88 101.31 2.62 2.73 94.97 7.05 7.81 100.51 5.19 5.43 99.78 2.95 3.11
216 Methiocarb-sulfoxide 13.23 88.78 5.90 6.99 104.86 6.82 6.84 104.54 6.17 6.21 101.82 5.30 5.48 96.86 3.94 4.28
217 Methomyl 7.40 108.31 5.15 5.01 93.67 7.23 8.12 98.37 5.92 6.33 101.47 2.36 2.45
218 Methoxyfenozide 9.06 101.82 3.15 3.25 91.64 7.20 8.27 102.14 3.70 3.81 100.27 3.12 3.28
219 Metoxychlor 10.18 99.59 3.79 4.00 97.39 6.35 6.86 102.08 3.77 3.89 98.23 3.26 3.49
220 Metrafenone 54.30 109.03 19.34 18.67 86.42 18.34 22.34 101.53 19.54 20.25 105.46 18.82 18.79
221 Metronidazole 11.22 97.19 11.15 12.07 103.48 4.54 4.62 97.54 5.86 6.33 99.29 6.04 6.40 100.33 3.86 4.05
222 Mevinphos (phosdrin) 14.05 88.35 12.61 15.02 114.31 1.58 1.46 104.46 7.37 7.42 103.89 5.30 5.37 95.13 3.47 3.83
223 Mirex 11.87 111.14 9.41 8.91 90.78 6.53 7.57 97.50 7.31 7.89 102.24 3.83 3.94
224 Monocrotophos 6.77 111.72 7.23 6.81 92.90 9.23 10.46 99.61 3.94 4.16 100.46 2.32 2.43
225 Moxidectin 41.02 98.76 13.82 14.73 103.02 14.72 15.04 88.79 12.89 15.28 97.74 17.16 18.48 99.42 14.08 14.91
226 Myclobutanil 6.85 110.18 3.93 3.76 92.89 9.45 10.71 100.33 5.38 5.65 100.68 2.32 2.43
227 N-(2,4-dimethylphenyl)-N’-methylformamidine (DMPF, metabolite of amitraz) 42.13 106.14 14.98 14.85 89.18 9.08 10.72 99.36 14.87 15.75 101.61 14.59 15.11
228 N,N-Dimethyl-N’-p-tolylsulphamide (DMST, metabolite of tolyfluanid) 10.56 97.35 10.02 10.83 104.27 7.42 7.49 98.60 6.49 6.93 98.66 6.22 6.64 100.29 3.64 3.82
229 Naphtalene 18.07 104.69 24.28 24.42 84.22 12.02 15.02 91.04 21.60 24.98 105.57 5.04 5.02
230 Naproxen 18.08 104.76 11.99 12.05 97.40 2.15 2.32 100.44 6.23 6.53
231 Novobiocin 23.78 86.15 21.57 24.36 101.53 6.13 6.35 101.37 8.19 8.51
232 Nuarimol 21.37 95.42 14.07 15.53 114.10 20.37 18.79 96.41 18.11 19.77 97.46 10.74 11.60 101.04 7.36 7.67
233 Ofurace 44.92 99.42 7.14 7.56 104.81 7.72 7.75 90.11 11.50 13.43 100.46 18.07 18.94 102.96 15.57 15.92
234 Omethoate 8.16 104.84 7.41 7.44 91.49 6.43 7.40 98.85 4.19 4.46 102.14 2.42 2.49
235 Oxadixyl 9.41 97.67 5.38 5.80 95.25 8.26 9.12 101.81 5.13 5.30 99.40 3.21 3.39
236 Oxamyl 4.96 109.00 5.35 5.17 99.81 5.00 5.28 94.77 5.40 6.00 102.24 4.17 4.30 99.23 1.62 1.72
237 Oxfendazole 14.43 112.00 9.85 9.26 98.20 2.86 3.06 93.13 4.89 5.53 100.75 7.35 7.68 100.63 4.97 5.19
238 Oxolinic acid 8.60 103.85 4.00 4.05 91.68 5.27 6.06 101.15 4.74 4.93 100.96 2.90 3.02
239 Oxydemeton methyl 22.47 102.56 5.85 6.00 92.13 4.64 5.30 99.17 6.15 6.52 101.58 7.73 8.01
240 Oxyfluorfen 26.60 107.15 18.84 18.51 101.78 18.11 18.73 93.71 22.54 24.32 94.68 10.13 11.27 104.32 8.85 8.93
241 Paclobutrazol 29.94 90.31 18.73 21.83 109.85 19.35 18.55 90.96 14.91 17.25 97.89 11.80 12.68 102.25 10.31 10.62
242 Parathion methyl 19.48 98.41 18.23 19.50 104.65 3.64 3.66 91.06 13.26 15.33 97.15 16.56 17.94 104.95 5.92 5.94
243 PCB 28 30.59 90.80 12.67 14.68 106.28 3.43 3.40 95.75 18.66 20.51 97.36 13.88 15.01 101.58 10.56 10.95
244 PCB 52 49.53 96.76 16.68 18.14 110.07 5.96 5.70 91.27 15.70 18.11 100.93 19.12 19.94 105.86 17.06 16.97
245 PCB 77 32.20 103.38 16.60 16.90 102.27 10.81 11.12 98.20 19.63 21.04 97.88 11.57 12.44 102.22 11.11 11.44
246 PCB 81 52.37 108.02 16.73 16.30 103.90 18.60 18.85 89.56 16.73 19.66 87.59 12.33 14.81 102.26 21.67 22.31
247 PCB 101 42.27 87.04 19.39 23.45 109.17 8.10 7.81 92.00 20.82 23.83 95.80 7.97 8.75 103.43 14.62 14.87
248 PCB 105 27.37 99.26 7.43 7.87 100.33 13.58 14.24 92.72 13.12 14.89 93.12 17.28 19.53 105.20 8.95 8.96
249 PCB 114 24.13 103.71 20.87 21.19 94.46 12.18 13.57 91.10 16.36 18.91 96.99 17.69 19.20 102.77 8.20 8.40
250 PCB 118 28.15 97.19 13.12 14.21 99.86 5.10 5.37 92.76 20.78 23.58 96.30 8.30 9.07 102.29 9.68 9.96
251 PCB 123 31.62 101.08 13.85 14.43 100.49 5.75 6.02 95.08 19.70 21.81 94.75 14.61 16.24 102.61 10.88 11.16
252 PCB 126 19.28 96.17 18.84 20.62 107.21 20.06 19.70 94.36 17.42 19.43 96.66 12.75 13.88 102.60 6.48 6.65
253 PCB 138 26.55 96.29 8.95 9.78 100.71 15.36 16.05 93.60 17.01 19.12 97.66 12.37 13.33 100.79 9.16 9.57
254 PCB 153 33.56 92.09 6.60 7.55 101.91 15.13 15.63 95.55 16.13 17.76 98.44 15.61 16.69 101.60 11.60 12.02
255 PCB 156 55.52 89.30 5.79 6.82 104.11 17.82 18.02 92.53 17.92 20.38 101.92 21.37 22.07 99.35 18.94 20.07
256 PCB 157 26.85 95.13 17.25 19.09 104.76 13.27 13.33 89.85 15.11 17.71 102.60 16.72 17.16 99.44 9.21 9.75
257 PCB 167 51.81 113.98 21.88 20.21 99.57 17.14 18.12 87.57 13.30 15.99 94.35 18.40 20.53 93.21 16.57 18.72
258 PCB 169 52.09 101.60 18.21 18.86 103.24 8.55 8.72 85.44 9.25 11.40 90.15 20.58 24.03 97.16 17.56 19.02
259 PCB 180 13.23 104.96 14.37 14.41 106.93 9.30 9.15 88.67 14.22 16.88 93.69 14.56 16.36 100.90 4.53 4.73
260 PCB 189 25.16 103.03 10.15 10.37 100.28 19.19 20.14 89.16 12.30 14.52 93.67 9.90 11.13 104.12 8.36 8.45
261 Penconazole 34.16 95.70 12.80 14.08 115.85 4.50 4.09 95.53 13.40 14.76 93.08 11.71 13.24 99.44 11.72 12.41
262 Pencycuron 20.48 98.16 9.03 9.69 105.55 4.45 4.43 96.26 4.83 5.28 100.53 7.15 7.49 100.12 7.06 7.42
263 Pendimethalin 17.70 90.91 14.47 16.76 105.21 7.43 7.43 99.02 3.67 3.90 102.02 5.04 5.20 97.75 5.82 6.27
264 Penicilina V 26.71 96.64 5.84 6.36 97.01 8.57 9.30 101.26 9.22 9.58
265 Permethrin 36.34 105.69 14.94 14.88 95.27 21.90 24.20 90.29 19.06 22.22 97.91 12.29 13.21
266 Phenanthrene 17.45 98.02 12.31 13.22 99.55 12.44 13.16 93.48 13.10 14.75 93.74 12.82 14.39 103.69 5.55 5.63
267 Phenylbutazone 49.13 91.74 15.73 18.05 93.57 19.01 21.39 105.65 16.94 16.87
268 Phosalone 11.29 100.31 7.80 8.18 102.56 5.32 5.47 94.92 4.35 4.82 99.26 7.11 7.54 100.09 3.89 4.09
269 Phosmet 13.71 104.01 7.48 7.57 98.61 6.23 6.65 103.07 4.47 4.56 97.45 4.32 4.67
270 Phosmet-oxon 7.06 97.85 4.69 5.05 97.35 8.44 9.13 102.67 5.14 5.27 98.02 1.99 2.13
271 Pirimicarb 10.35 92.13 7.98 9.12 108.26 1.33 1.29 103.45 4.95 5.04 103.13 3.94 4.02 95.99 2.20 2.42
272 Pirimicarb-desmethyl 8.59 102.89 7.11 7.27 101.86 3.08 3.18 96.80 6.76 7.35 101.82 3.15 3.26 98.62 2.78 2.97
273 Pirimiphos ethyl 49.06 92.82 19.20 21.77 118.12 2.68 2.39 87.29 11.06 13.34 96.72 14.11 15.36 110.86 15.95 15.15
274 Pirimiphos methyl 46.53 97.86 11.37 12.23 106.89 1.77 1.74 91.79 11.32 12.99 101.94 17.14 17.69 107.79 15.68 15.32
275 Prochloraz 11.75 93.09 13.04 14.74 109.38 9.57 9.21 104.39 6.98 7.03 103.14 5.34 5.45 95.40 2.45 2.71
276 Procymidone 47.71 106.77 7.90 7.79 88.94 18.04 21.35 94.09 11.30 12.65 96.19 15.88 17.38
277 Profenofos 19.09 100.50 11.04 11.56 101.67 8.80 9.11 100.12 6.04 6.35 101.11 7.81 8.13 98.72 6.47 6.90
278 Propamocarb 5.99 103.07 4.64 4.74 87.68 3.95 4.75 100.88 3.74 3.90 101.51 1.80 1.86
279 Propargite 20.43 98.90 9.92 10.56 102.07 5.44 5.61 97.64 5.69 6.14 98.89 6.67 7.10 100.75 7.04 7.36
280 Propiconazole 12.75 96.84 8.80 9.57 100.37 8.04 8.43 100.50 5.91 6.19 98.02 4.13 4.43
281 Propoxur 7.88 106.77 12.22 12.05 100.74 5.19 5.42 95.66 6.74 7.42 102.83 4.63 4.74 99.26 2.65 2.81
282 Propyzamide (pronamide) 7.08 92.65 19.33 21.96 95.89 6.00 6.59 95.61 6.94 7.65 100.37 5.71 5.98 99.85 2.43 2.57
283 Proquinazid 20.15 93.83 12.24 13.73 108.78 6.04 5.85 101.24 7.90 8.22 102.34 6.01 6.18 96.68 6.44 7.01
284 Prothioconazol 20.98 99.10 11.03 11.71 111.77 11.21 10.56 101.24 15.30 15.91 101.44 7.09 7.36 100.39 7.23 7.58
285 Prothiophos 54.52 99.76 20.17 21.29 115.45 19.52 17.79 90.43 16.79 19.54 92.15 10.78 12.31 106.16 18.85 18.69
286 Pymetrozine 12.11 104.52 9.45 9.52 99.96 6.47 6.81 98.85 7.40 7.88 100.89 4.14 4.32
287 Pyraclostrobin 14.46 92.85 6.84 7.76 103.95 2.37 2.40 97.43 5.66 6.11 100.22 6.57 6.90 100.04 4.98 5.24
288 Pyrazophos 13.83 97.27 7.18 7.77 104.11 8.90 9.00 100.36 6.58 6.90 100.04 5.66 5.96 99.70 4.75 5.02
289 Pyrene 35.48 84.48 4.35 5.42 118.27 15.20 13.53 90.78 10.35 12.00 95.73 8.21 9.03 102.81 12.24 12.53
290 Pyridaben 21.92 99.30 12.16 12.89 102.10 3.57 3.68 97.39 5.95 6.43 99.28 7.39 7.83 100.30 7.56 7.93
291 Pyridaphenthion 13.23 100.15 9.50 9.99 101.73 5.42 5.61 96.49 3.96 4.32 100.26 4.92 5.17 99.95 4.55 4.80
292 Pyrimethanil 21.20 95.66 16.08 17.69 105.17 12.00 12.01 91.20 11.13 12.84 94.12 12.46 13.94 103.96 6.91 6.99
293 Pyriproxifen 17.64 96.87 4.83 5.25 105.33 2.02 2.02 98.71 5.79 6.18 97.28 5.56 6.01 91.30 0.94 1.09
294 Quinalfos 11.63 94.48 10.56 11.76 96.90 6.47 7.03 106.43 6.56 6.49 101.72 6.64 6.87 96.67 3.22 3.51
295 Quinoxyfen 17.58 90.90 11.93 13.81 100.16 8.47 8.90 102.02 7.55 7.79 102.26 5.09 5.24 96.99 5.60 6.07
296 Rifampicin 38.32 95.11 8.51 9.42 99.82 8.14 8.58 99.31 13.14 13.93
297 Rotenone 38.71 116.09 14.12 12.80 101.14 19.83 20.64 103.06 11.26 11.50 95.90 12.74 13.98
298 Roxithromycin 16.85 105.39 12.55 12.54 90.66 7.64 8.87 96.26 3.89 4.25 103.64 5.33 5.41
299 Simazine 5.25 106.22 13.48 13.35 95.00 4.14 4.59 93.84 6.29 7.06 101.60 4.45 4.61 99.67 1.79 1.89
300 Spinosad (two isomers) 22.35 105.88 7.75 7.70 106.76 13.25 13.05 100.51 6.11 6.45 97.07 7.36 7.88
301 Spiramycin (two isomers) 6.56 95.12 6.27 6.94 98.30 4.51 4.83 101.25 2.10 2.19
302 Spirodiclofen 15.03 105.95 10.56 10.49 96.95 4.55 4.94 100.27 5.18 5.44
303 Spiromesifen 12.81 101.56 4.83 5.00 99.43 6.18 6.54 97.60 5.75 6.20 100.24 4.41 4.63
304 Spiroxamine 11.53 84.84 7.85 9.74 105.10 1.89 1.90 104.57 7.11 7.15 102.72 4.87 4.99 96.16 2.90 3.17
305 Strychnine 11.90 98.61 6.60 7.04 92.65 8.23 9.35 101.86 5.04 5.21 100.73 4.08 4.27
306 Sulfacetamide 18.66 95.38 12.81 14.13 101.54 7.67 7.95 100.85 6.43 6.71
307 Sulfachloropiridacine 4.66 96.98 0.49 0.53 92.42 5.44 6.19 99.53 3.02 3.20 100.56 1.56 1.64
308 Sulfadiacine 22.38 108.52 15.90 15.42 91.45 5.34 6.15 97.90 5.89 6.33 102.45 7.61 7.82
309 Sulfadimetoxine 10.71 110.25 12.55 11.99 96.34 4.79 5.24 96.18 5.92 6.47 100.38 6.04 6.34 100.47 3.68 3.86
310 Sulfadoxine 7.31 107.49 7.96 7.79 94.89 5.76 6.39 94.43 6.42 7.16 102.25 5.28 5.44 99.73 2.51 2.64
311 Sulfameracine 6.60 103.87 2.73 2.77 94.75 4.37 4.85 100.53 7.96 8.33 100.38 2.26 2.37
312 Sulfametacine 8.13 105.16 1.02 1.02 92.79 8.30 9.42 100.18 5.58 5.86 100.61 2.78 2.90
313 Sulfametizole 4.48 105.55 4.45 4.44 94.95 7.79 8.64 102.75 5.57 5.71 99.45 1.49 1.58
314 Sulfametoxazole 9.86 105.88 3.94 3.92 93.12 8.76 9.90 103.21 4.47 4.56 98.89 3.29 3.50
315 Sulfametoxipiridacine 10.11 103.07 3.90 3.99 89.72 6.58 7.72 101.01 5.53 5.76 100.77 3.46 3.61
316 Sulfamonomethoxine 30.69 120.10 11.58 10.15 93.43 9.85 11.10 100.65 5.38 5.63 100.77 10.60 11.07
317 Sulfapyridine 13.16 107.39 7.54 7.39 95.05 7.02 7.77 98.88 7.30 7.77 101.09 4.49 4.68
318 Sulfaquinoxaline 19.01 108.10 8.28 8.06 92.03 6.07 6.95 98.12 7.23 7.76 102.11 6.45 6.65
319 Sulfatiazole 13.98 107.25 18.23 17.89 91.67 8.92 10.24 100.18 10.87 11.42 100.13 4.82 5.06
320 Sulfisoxazole 6.76 95.64 5.52 6.08 90.14 5.37 6.27 101.96 3.79 3.91 99.82 2.32 2.45
321 Tebuconazole 4.02 96.70 9.65 10.50 96.71 8.87 9.65 100.97 5.13 5.35 99.07 1.22 1.30
322 Tebufenocide 9.66 98.70 9.29 9.90 103.48 4.98 5.07 100.37 9.81 10.29 98.74 6.14 6.55 100.66 3.31 3.46
323 Tebufenpyrad 54.25 98.40 19.31 20.65 103.42 14.26 14.51 87.22 16.18 19.53 96.43 16.30 17.80 93.97 17.61 19.73
324 Teflubenzuron 14.59 103.61 16.19 16.45 91.96 11.61 13.29 99.92 10.40 10.96 100.04 5.03 5.29
325 Tefluthrin 18.98 94.50 18.42 20.52 109.30 5.13 4.94 95.83 13.31 14.62 97.15 10.26 11.12 103.00 6.29 6.43
326 Telodrin (isobenzan) 31.11 93.25 19.35 21.84 116.61 15.64 14.12 89.63 17.21 20.21 94.46 10.00 11.14 104.86 10.43 10.47
327 Terbufos 17.89 89.87 18.10 21.20 101.84 16.58 17.14 98.77 16.02 17.07 99.46 14.72 15.58 105.00 5.24 5.25
328 Terbuthylazine 14.43 93.29 4.25 4.80 109.08 4.95 4.78 96.04 4.63 5.07 98.95 5.77 6.14 100.31 4.97 5.22
329 Tetrachlorvinphos 15.02 86.68 16.44 19.97 104.08 5.78 5.84 103.29 9.75 9.93 100.97 4.69 4.89 96.47 4.48 4.89
330 Tetraconazole 38.67 89.01 16.15 19.10 114.33 10.30 9.48 94.97 19.82 21.97 99.62 11.36 12.01 106.33 12.98 12.85
331 Tetradifon 21.58 92.25 17.26 19.70 108.82 9.05 8.75 97.26 10.04 10.87 98.91 10.35 11.02 99.23 7.38 7.83
332 Tetramethrin 38.36 110.19 8.77 8.38 87.06 11.18 13.51 99.88 13.15 13.85 96.19 12.68 13.88
333 Thiabendazole 6.96 109.34 8.89 8.56 99.89 4.64 4.89 92.53 7.57 8.61 102.95 3.30 3.37 99.44 2.36 2.50
334 Thiacloprid 7.62 100.27 9.33 9.79 99.72 2.71 2.86 96.75 5.67 6.17 102.32 4.32 4.44 98.86 2.49 2.65
335 Thiamethoxam 8.90 94.30 9.01 10.05 101.19 2.45 2.55 99.73 3.06 3.23
336 Thiophanate methyl 9.82 94.93 7.65 8.49 102.70 1.97 2.02 100.03 5.00 5.27 101.78 5.03 5.20 97.82 3.00 3.22
337 Tolclofos methyl 18.85 96.49 2.19 2.39 93.05 7.46 8.44 104.27 5.91 5.97
338 Tolfenamic acid 15.70 96.60 20.72 22.58 113.09 5.70 5.31 93.69 11.93 13.40 95.77 17.20 18.90 101.95 5.29 5.46
339 Triadimefon 15.86 103.69 22.53 24.92 96.37 21.63 23.62 97.25 7.36 7.97 100.42 5.47 5.73
340 Triadimenol 11.21 90.21 16.68 19.46 108.01 10.30 10.04 104.18 2.94 2.97 102.84 6.90 7.07 95.94 2.60 2.86
341 Triazophos (hostathion) 11.28 107.10 15.08 14.83 96.40 6.06 6.62 100.08 4.21 4.43 99.92 3.88 4.09
342 Trichlorfon 11.09 97.09 8.26 8.96 103.21 3.75 3.82 97.44 5.31 5.74 99.08 5.57 5.92 100.42 3.82 4.00
343 Trifloxystrobin 7.09 94.36 14.78 16.49 96.83 5.76 6.26 98.87 4.98 5.31 100.65 2.41 2.52
344 Triflumizole 14.95 98.38 11.61 12.43 99.91 3.85 4.05 97.81 6.89 7.41 99.87 5.89 6.21 100.10 5.15 5.42
345 Triflumuron 10.52 97.57 4.93 5.32 100.94 4.59 4.79 97.95 7.98 8.58 99.43 5.30 5.62 100.20 3.62 3.81
346 Trifluralin 18.05 94.40 16.87 18.82 95.90 6.43 7.05 103.36 7.85 8.00 97.05 5.78 6.27
347 Trimethoprim 47.12 112.07 12.04 11.31 96.24 11.78 12.88 101.74 20.93 21.65 108.42 15.79 15.33
348 Triticonazole 10.27 105.14 4.25 4.26 95.26 6.47 7.15 96.56 7.30 7.96 102.90 2.96 3.03
349 Tylmicosin 10.97 113.79 16.19 14.98 88.65 6.89 8.18 101.93 6.09 6.29 99.54 3.75 3.97
350 Tylosin 10.56 107.72 11.23 10.98 96.69 5.96 6.49 99.51 5.98 6.32 100.64 3.62 3.79
351 Vinclozolin 18.23 87.26 12.21 14.73 113.36 11.73 10.89 98.12 18.88 20.25 96.44 12.88 14.06 102.62 6.09 6.25
352 Warfarin 10.77 87.78 17.57 21.07 91.37 23.07 24.58 95.23 6.45 7.13 102.69 4.32 4.43 98.14 3.45 3.70
353 Zoxamide 17.19 80.27 12.78 16.76 100.65 7.00 7.33 106.21 9.24 9.16 103.64 7.51 7.62 94.40 4.35 4.85
Blank cells were set for compounds that have a higher LOQ than the lowest concentrations tested.