Table 1. Optimum Furnace Program of GFAAS.
step | temperature (°C) | time (s) | Ar flow rate (L min–1) |
---|---|---|---|
dry | |||
1 | 85 | 5 | 0.3 |
2 | 95 | 40 | 0.3 |
3 | 120 | 10 | 0.3 |
pyrolysis | |||
1 | 400 | 5 | 0.3 |
2 | 400 | 1 | 0.3 |
3 | 400 | 2 | 0.0 |
atomization | |||
1 | 2100 | 1 | 0.0 |
2 | 2100 | 2 | 0.0 |
3 | 2100 | 2 | 0.3 |