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. 2023 May 25;10(Pt 4):430–436. doi: 10.1107/S2052252523004141

Table 1. MicroED statistics of proteinase K crystallized by suspended drop (PDB entry 8sdk and EMD-40351).

Data collection
Accelerating voltage (kV) 300
Wavelength (Å) 0.019687
Electron source Field emission gun
Total accumulated exposure (e Å−2) 0.64
No. of crystals 1
Microscope Thermo Fisher Titan Krios
Camera Falcon 4 electron counting
Rotation rate (° s−1) 0.2
 
Data analysis
Resolution range (Å) 30.42–2.10
Space group P43212
a, b, c (Å) 68.26, 68.26, 101.95
α, β, γ (°) 90, 90, 90
Total/unique reflections 56301/12774
Multiplicity 4.41
Completeness (%) 87.0
Mean I/Iσ(I) 2.82
CC 1/2 92.5
R work 0.2442
R free 0.2917