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. 2023 Jun 15;30(Pt 4):841–846. doi: 10.1107/S160057752300406X

Table 2. Selective refinement statistics for L-threonine and tHEWL collected using laboratory and synchrotron data.

Comparable laboratory and synchrotron data are only available for L-threonine.

  L-Threonine tHEWL
X-ray source Synergy-S Synergy-S MX1 LTHREO21 MX1 3LYM 4WLD§
Pressure (GPa) Ambient 0.15 0.15 Ambient 0.44 0.1 0.0001
Completeness (%) 100 51.2 44.7 100 63.2 N/A N/A
Resolution 0.73 0.80 0.76 N/A 2.10 2.00 1.54
I 26.7 31.9 54.6 N/A 7.0 N/A N/A
R 1 (%) 3.95 4.04 4.04 2.60 21.7 14.9 15.0
Data collection time (s) 2337 9504 14 N/A 70 N/A N/A
Space group P212121 P212121 P212121 P212121 P43212 P43212 P43212
a (Å) 5.1456 (2) 5.1419 (2) 5.1498 (5) 5.1481 (1) 79.045 78.69 79.197
b (Å) 7.7415 (4) 7.7217 (4) 7.7304 (5) 7.7426 (1) 79.045 78.69 79.197
c (Å) 13.6223 (6) 13.613 (5) 13.602 (6) 13.6138 (2) 37.865 38 37.9
V3) 542.64 (4) 540.5 (2) 541.4 (3) 542.642 (15) 236585 235300 237715

CSD reference = LTHREO21 (Giordano et al., 2019).

PDB reference = 3lym (Kundrot & Richards, 1987).

§

PDB reference = 4wld (Yamada et al., 2015).