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. 2023 Jun 22;25(26):4862–4867. doi: 10.1021/acs.orglett.3c01660

Table 2. Giese Reaction between Compounds 1a1e and 2a2ea.

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a

Reaction conditions: compounds 1a1d (1 equiv, 0.12 mmol), compounds 2a2e (2 equiv, 0.24 mmol), DIPEA (3 equiv, 0.36 mmol), HE (2 equiv, 0.24 mmol), photocatalyst D (5 mol %, 0.006 mmol), ACN/H2O (2:1, 1 mL), blue LED (10 W), and time of 2 h. dr was calculated by NMR on the crude, and yield was calculated after the chromatography column.